ETHYL 2-CYANO-3-(3-PYRIDINYL)ACRYLATE

Base Information

• Chemical Name: ETHYL 2-CYANO-3-(3-PYRIDINYL)ACRYLATE
• CAS No.: 103011-95-6
• Molecular Formula: C11H10N2O2
• Molecular Weight: 202.20900
• Hs Code.: 2933399090
• Mol file: 103011-95-6.mol

Synonyms:2-Propenoic acid,2-cyano-3-(3-pyridinyl)-,ethyl ester,(2E);ethyl 2-cyano-3-(3-pyridinyl)acrylate;ethyl (E)-2-cyano-3-(3-pyridyl)-2-propenoate;2-cyano-3-pyridin-3-yl-acrylic acid ethyl ester;ethyl 2-cyano-3-(3-pyridyl)-(E)-2-propenoate;Ethyl 2-cyano-3-(pyridin-3-yl)acrylate;ethyl (2E)-2-cyano-3-(3-pyridinyl)-2-propenoate;2-Cyan-3-[3]pyridyl-acrylsaeure-aethylester;2-cyano-3-[3]pyridyl-acrylic acid ethyl ester;

Chemical Property of ETHYL 2-CYANO-3-(3-PYRIDINYL)ACRYLATE

Chemical Property:

• Melting Point: 67-70°C
• PSA: 62.98000
• LogP: 1.55168

Purity/Quality:

98%min ^*data from raw suppliers

Ethyl2-Cyano-3-(3-pyridyl)acrylate ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 2-CYANO-3-(3-PYRIDINYL)ACRYLATE

There total 3 articles about ETHYL 2-CYANO-3-(3-PYRIDINYL)ACRYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-pyridinecarboxaldehyde (500-22-1) + ethyl 2-cyanoacetate (105-56-6) → ethyl 2-cyano-3-(3-pyridyl)-(E)-2-propenoate (17999-71-2,103011-95-6,136633-60-8)

Guidance literature:

ytterbium(III) perfluorooctanesulfonate; In toluene; at 80 ℃; for 3h;

DOI:10.1080/00304940709458582

Reference yield:

piperidine (110-89-4) + 3-pyridinecarboxaldehyde (500-22-1) + ethyl 2-cyanoacetate (105-56-6) → ethyl 2-cyano-3-(3-pyridyl)-(E)-2-propenoate (17999-71-2,103011-95-6,136633-60-8)

Guidance literature:

In ethanol; water; acetic acid;

Reference yield:

→ ethyl 2-cyano-3-(3-pyridyl)-(E)-2-propenoate (17999-71-2,103011-95-6,136633-60-8)

Guidance literature:

Nicotinaldehyd, Cyanessigsaeure-ethylester, A., wenig Piperidin;

upstream raw materials:

3-pyridinecarboxaldehyde

ethyl 2-cyanoacetate

piperidine