C₂₉H₄₇NO₅

Base Information

Chemical Name:C₂₉H₄₇NO₅
CAS No.:1417141-65-1
Molecular Formula:C₂₉H₄₇NO₅
Molecular Weight:489.696
Hs Code.:

C<sub>29</sub>H<sub>47</sub>NO<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₄₇NO₅

Chemical Property:

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Technology Process of C₂₉H₄₇NO₅

There total 2 articles about C₂₉H₄₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417141-58-2
benzyl (4R,5R)-4-allyl-2,2-dimethyl-1,3-dioxan-5-ylcarbamate

: 56221-91-1
(Z)-Δ¹³-tetradecenyl acetate

: 1417141-65-1
C₂₉H₄₇NO₅

: 1417141-67-3
C₂₉H₄₇NO₅

Guidance literature:: benzyl (4R,5R)-4-allyl-2,2-dimethyl-1,3-dioxan-5-ylcarbamate; (Z)-Δ¹³-tetradecenyl acetate; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere; Reflux;

With sodium methylate; In methanol; at 20 ℃; for 2h; Overall yield = 51 %; Overall yield = 580 mg;
DOI:10.1021/jo302355t

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1417141-65-1
C₂₉H₄₇NO₅

: 1417141-67-3
C₂₉H₄₇NO₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: indium / water; 1,4-dioxane / 20 h / 100 °C

1.2: 24 h / 10 - 20 °C / pH 7 - 8

2.1: sodium periodate / water; 1,4-dioxane / 3 h / 5 - 20 °C

2.2: 5 °C

2.3: 5 h / 20 °C

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Reflux

3.2: 2 h / 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; indium; sodium periodate; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo302355t