1-phenylethyldimesitylborane

Base Information

Chemical Name:1-phenylethyldimesitylborane
CAS No.:74178-60-2
Molecular Formula:C₂₆H₃₁B
Molecular Weight:354.343
Hs Code.:

Synonyms:

Suppliers and Price of 1-phenylethyldimesitylborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenylethyldimesitylborane

Chemical Property:

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Technology Process of 1-phenylethyldimesitylborane

There total 1 articles about 1-phenylethyldimesitylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74178-59-9
benzyldimesitylborane

: 77-78-1
dimethyl sulfate

: 74178-60-2
1-phenylethyldimesitylborane

Guidance literature:: With lithium dicyclohexylamide; In tetrahydrofuran; (N2); borane was added to stirred soln. of LiN(C6H11)2 at room temp., mixt. was stirred for 3 h, then stoich. amt. of DMS was added; THF was distd. off, ether was added and mixt. extd. with dilute citric acid soln., ether layer washed with H2O and dried (MgSO4); ether was removed in vac., residue recrystd. from MeOH; elem. anal.;
DOI:10.1016/S0022-328X(00)82409-2

Reference yield:

: 74178-60-2
1-phenylethyldimesitylborane

: 77-78-1
dimethyl sulfate

: 74178-61-3
2-phenyl-prop-2-yldimesitylborane

Guidance literature:: With lithium dicyclohexylamide; In tetrahydrofuran; (N2); borane was added to stirred soln. of LiN(C6H11)2 at room temp., mixt. was stirred for 20 h, then stoich. amt. of DMS was added; THF was distd. off, ether was added and mixt. extd. with dilute citric acid soln., ether layer washed with H2O and dried (MgSO4); ether was removed in vac., residue recrystd. from MeOH; elem. anal.;
DOI:10.1016/S0022-328X(00)82409-2