4-benzyloxymethoxy-3-hydroxy-1,4-diphenylbutan-1-one

Base Information

Chemical Name:4-benzyloxymethoxy-3-hydroxy-1,4-diphenylbutan-1-one
CAS No.:98215-34-0
Molecular Formula:C₂₄H₂₄O₄
Molecular Weight:376.452
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-benzyloxymethoxy-3-hydroxy-1,4-diphenylbutan-1-one

Chemical Property:

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Technology Process of 4-benzyloxymethoxy-3-hydroxy-1,4-diphenylbutan-1-one

There total 6 articles about 4-benzyloxymethoxy-3-hydroxy-1,4-diphenylbutan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4358-87-6
(RS)-methyl mandelate

: 98215-34-0,98215-40-8
4-benzyloxymethoxy-3-hydroxy-1,4-diphenylbutan-1-one

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / silver oxide, calcium chloride / Heating

2: 83 percent

3: 1.) LiAlH₄, 2.) Swern oxidation

4: 1.) N-BuLi, HMPA / tetrahydrofuran / 1 h / -50 °C

5: Na/Hg, NaH₂PO₄ / methanol / -20 °C

6: Cu²⁺

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium dihydrogenphosphate; sodium amalgam; lithium aluminium tetrahydride; n-butyllithium; copper(II) ion; calcium chloride; silver(l) oxide; In tetrahydrofuran; methanol;

Reference yield:

: 3558-61-0
methyl 2-methoxy-2-phenylacetate

: 98215-34-0,98215-40-8
4-benzyloxymethoxy-3-hydroxy-1,4-diphenylbutan-1-one

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent

2: 1.) LiAlH₄, 2.) Swern oxidation

3: 1.) N-BuLi, HMPA / tetrahydrofuran / 1 h / -50 °C

4: Na/Hg, NaH₂PO₄ / methanol / -20 °C

5: Cu²⁺

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium dihydrogenphosphate; sodium amalgam; lithium aluminium tetrahydride; n-butyllithium; copper(II) ion; In tetrahydrofuran; methanol;

Reference yield:

: 98215-11-3
O-benzyloxymethyl(phenyl)glycolaldehyde

: 98215-34-0,98215-40-8
4-benzyloxymethoxy-3-hydroxy-1,4-diphenylbutan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N-BuLi, HMPA / tetrahydrofuran / 1 h / -50 °C

2: Na/Hg, NaH₂PO₄ / methanol / -20 °C

3: Cu²⁺

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium dihydrogenphosphate; sodium amalgam; n-butyllithium; copper(II) ion; In tetrahydrofuran; methanol;