C₂₂H₂₆N₂O₆

Base Information

• Chemical Name: C₂₂H₂₆N₂O₆
• CAS No.: 78094-99-2
• Molecular Formula: C₂₂H₂₆N₂O₆
• Molecular Weight: 414.458
• Mol file: 78094-99-2.mol

Synonyms:

Chemical Property of C₂₂H₂₆N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₆N₂O₆

There total 5 articles about C₂₂H₂₆N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

C15H24O (78094-98-1) + 3,5-dinitrobenoyl chloride (99-33-2) → C22H26N2O6 (78094-99-2)

Guidance literature:

In pyridine; 1.) 50 deg C, 10 min, 2.) room temperature, 30 min;

DOI:10.1039/P19810000995

Reference yield:

sesquifilifolone (64125-53-7,72581-35-2) → C22H26N2O6 (78094-99-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 7 percent / sodium borohydride / methanol / 2 h / 0 °C

2: 30 percent / 50percent aq. sulphuric acid / diethyl ether

3: 1.) diborane, 2.) 3M aq. sodium hydroxide, 30percent hydrogen peroxide / 1.) tetrahydrofuran, room temperature, 2 h, 2.) room temperature, 30 min, 50 deg C, 30 min

4: 71 percent / pyridine / 1.) 50 deg C, 10 min, 2.) room temperature, 30 min

With sodium hydroxide; sodium tetrahydroborate; sulfuric acid; dihydrogen peroxide; diborane; In pyridine; methanol; diethyl ether;

DOI:10.1039/P19810000995

Reference yield:

C15H22 (78094-97-0) → C22H26N2O6 (78094-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) diborane, 2.) 3M aq. sodium hydroxide, 30percent hydrogen peroxide / 1.) tetrahydrofuran, room temperature, 2 h, 2.) room temperature, 30 min, 50 deg C, 30 min

2: 71 percent / pyridine / 1.) 50 deg C, 10 min, 2.) room temperature, 30 min

With sodium hydroxide; dihydrogen peroxide; diborane; In pyridine;

DOI:10.1039/P19810000995

upstream raw materials:

C₁₅H₂₄O

3,5-dinitrobenoyl chloride

C₁₅H₂₂

sesquifilifolone