3-(n-butyl 2-methylsuccinoyl)-4-dimethyl-t-butylsilyloxymethyl 1-styryl-1,8-dihydroazocine

Base Information

Chemical Name:3-(n-butyl 2-methylsuccinoyl)-4-dimethyl-t-butylsilyloxymethyl 1-styryl-1,8-dihydroazocine
CAS No.:83253-66-1
Molecular Formula:C₃₁H₄₅NO₄Si
Molecular Weight:523.788
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(n-butyl 2-methylsuccinoyl)-4-dimethyl-t-butylsilyloxymethyl 1-styryl-1,8-dihydroazocine

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Technology Process of 3-(n-butyl 2-methylsuccinoyl)-4-dimethyl-t-butylsilyloxymethyl 1-styryl-1,8-dihydroazocine

There total 6 articles about 3-(n-butyl 2-methylsuccinoyl)-4-dimethyl-t-butylsilyloxymethyl 1-styryl-1,8-dihydroazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 26481-88-9
1-styryl-1,2-dihydropyridine

: 83253-55-8
n-butyl 2-methyl-4-oxo-7-dimethyl-t-butylsilyloxyhept-5-ynoate

: 83253-66-1
3-(n-butyl 2-methylsuccinoyl)-4-dimethyl-t-butylsilyloxymethyl 1-styryl-1,8-dihydroazocine

Guidance literature:: In tetrahydrofuran; at 50 ℃; for 96h; under argon;
DOI:10.1016/0040-4020(82)80133-6

Reference yield:

: 5150-93-6
succinic anhydride monobutyl ester

: 83253-66-1
3-(n-butyl 2-methylsuccinoyl)-4-dimethyl-t-butylsilyloxymethyl 1-styryl-1,8-dihydroazocine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) lithium diisopropylamide, n-BuLi / 1.) THF, -78 deg C, 1 h; 2.) -78 deg C, 1 h

2: 78 percent / SOCl₂ / 3 h / 35 °C

3: 1.) AgNO₃, conc NH₄OH / 1.) water, MeOH, 25 deg C, 2 h; 2.) CCl₄, 4 h, heating

4: 34 percent / tetrahydrofuran / 96 h / 50 °C / under argon

With ammonium hydroxide; n-butyllithium; thionyl chloride; silver nitrate; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/0040-4020(82)80133-6

Reference yield:

: 76782-82-6
tert-Butyldimethyl(prop-2-ynyloxy)silane

: 83253-66-1
3-(n-butyl 2-methylsuccinoyl)-4-dimethyl-t-butylsilyloxymethyl 1-styryl-1,8-dihydroazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) AgNO₃, conc NH₄OH / 1.) water, MeOH, 25 deg C, 2 h; 2.) CCl₄, 4 h, heating

2: 34 percent / tetrahydrofuran / 96 h / 50 °C / under argon

With ammonium hydroxide; silver nitrate; In tetrahydrofuran;
DOI:10.1016/0040-4020(82)80133-6