Technology Process of 2,5-Dimethoxy-hydrochinon-di-
There total 1 articles about 2,5-Dimethoxy-hydrochinon-di- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Aus 2,5-Dimethoxy-hydrochinon u. Dihydropyran in abs. THF unter N2 bei 0grad in Ggw. v. wss.fr. Toluol-4-sulfonsaeure;
- Guidance literature:
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Multi-step reaction with 8 steps
1: (i) nBuLi, THF, Et2O, (ii) /BRN= 1900390/, (iii) aq. NaOH
2: K2CO3 / dimethylformamide
3: KOMe / methanol / Heating
4: (i) SOCl2, Py, THF, (ii) /BRN= 102415/, Et2O, benzene
5: benzene; diethyl ether
6: (i) aq. MeOH, (ii) aq. NaOH
7: H2 / PdO / ethanol
8: Ag2O, MgSO4 / benzene
With
potassium methanolate; hydrogen; magnesium sulfate; potassium carbonate; silver(l) oxide;
trimethyleneglycol;
In
methanol; diethyl ether; ethanol; N,N-dimethyl-formamide; benzene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: (i) nBuLi, THF, Et2O, (ii) /BRN= 1900390/, (iii) aq. NaOH
2: K2CO3 / dimethylformamide
3: KOMe / methanol / Heating
4: (i) SOCl2, Py, THF, (ii) /BRN= 102415/, Et2O, benzene
5: benzene; diethyl ether
6: (i) aq. MeOH, (ii) aq. NaOH
7: H2 / PdO / ethanol
With
potassium methanolate; hydrogen; potassium carbonate;
trimethyleneglycol;
In
methanol; diethyl ether; ethanol; N,N-dimethyl-formamide; benzene;