O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose

Base Information

• Chemical Name: O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose
• CAS No.: 96961-36-3
• Molecular Formula: C₈₄H₇₄N₂O₂₆
• Molecular Weight: 1527.51

Synonyms:

Chemical Property of O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose

Chemical Property:

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Useful:

Technology Process of O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose

There total 2 articles about O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

O-(3-O-acetyl-4,6-di-O-benzoyl-2-deoxy-2-phtalimido-β-D-glucopyranosyl)-(1<*>2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-4-O-benzoyl-1,2-O-<1-(exo-cyano)ethylidene>-β-L-rhamnopyranose (96961-32-9,102046-17-3) → O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose (96961-36-3,102046-18-4)

Guidance literature:

With methanol; acetyl chloride; In chloroform; at 20 ℃; for 3.5h;

DOI:10.1016/S0040-4020(01)96688-8

Reference yield: 8.6%

O-(3-O-acetyl-4,6-di-O-benzoyl-2-deoxy-2-phtalimido-β-D-glucopyranosyl)-(1<*>2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-4-O-benzoyl-1,2-O-<1-(exo-cyano)ethylidene>-β-L-rhamnopyranose (96961-32-9,102046-17-3) → O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose (96961-36-3,102046-18-4) + C85H77NO28 + C87H79NO29

Guidance literature:

With acetyl chloride; In methanol; chloroform; at 20 ℃; for 3.75h;

DOI:10.1007/BF01142799

Reference yield:

trityl perchlorate (16721-97-4) + O-(4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose (96961-36-3,102046-18-4) → O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose (96961-37-4,102046-21-9)

Guidance literature:

With 2,4,6-trimethyl-pyridine; In dichloromethane; for 0.25h;

DOI:10.1007/BF01142800

upstream raw materials:

O-(3-O-acetyl-4,6-di-O-benzoyl-2-deoxy-2-phtalimido-β-D-glucopyranosyl)-(1<*>2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1<*>3)-4-O-benzoyl-1,2-O-<1-(exo-cyano)ethylidene>-β-L-rhamnopyranose

Downstream raw materials:

O-(4,6-di-O-benzoyl-2-desoxy-3-O-trityl-2-phthalimido-β-D-glucopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4-di-O-benzoyl-α-L-rhamnopyranosyl)-(1->3)-4-O-benzoyl-1,2-O-<1-(exocyano)ethylidene>-β-L-rhamnopyranose

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