N4-[α-D-mannopyranosyl-(1->3)-[α-D-mannopyranosyl-(1->6)]-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl]-N2-(benzyloxycarbonyl)-L-asparagine methyl ester

Base Information

• Chemical Name: N4-[α-D-mannopyranosyl-(1->3)-[α-D-mannopyranosyl-(1->6)]-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl]-N2-(benzyloxycarbonyl)-L-asparagine methyl ester
• CAS No.: 1065009-06-4
• Molecular Formula: C₄₇H₇₂N₄O₃₀
• Molecular Weight: 1173.1

Synonyms:

Chemical Property of N4-[α-D-mannopyranosyl-(1->3)-[α-D-mannopyranosyl-(1->6)]-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl]-N2-(benzyloxycarbonyl)-L-asparagine methyl ester

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Technology Process of N4-[α-D-mannopyranosyl-(1->3)-[α-D-mannopyranosyl-(1->6)]-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl]-N2-(benzyloxycarbonyl)-L-asparagine methyl ester

There total 1 articles about N4-[α-D-mannopyranosyl-(1->3)-[α-D-mannopyranosyl-(1->6)]-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl]-N2-(benzyloxycarbonyl)-L-asparagine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

Nα-(benzyloxycarbonyl)-Nγ-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-L-asparagine O-methyl ester (199928-18-2) + 2-methyl-[α-D-mannopyranosyl-(1->3)-[α-D-mannopyranosyl-(1->6)]-β-D-glucopyranosyl-(1->4)-1,2-dideoxy-α-D-glucopyrano]-[2,1-d]oxazoline (1065008-93-6) → N4-[α-D-mannopyranosyl-(1->3)-[α-D-mannopyranosyl-(1->6)]-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranosyl]-N2-(benzyloxycarbonyl)-L-asparagine methyl ester (1065009-06-4)

Guidance literature:

With endohexosaminidase M; at 23 ℃; for 3h; pH=6.0; aq. phosphate buffer; Enzymatic reaction;

DOI:10.1002/chem.200800365

upstream raw materials:

Nα-(benzyloxycarbonyl)-Nγ-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-L-asparagine O-methyl ester

2-methyl-[α-D-mannopyranosyl-(1->3)-[α-D-mannopyranosyl-(1->6)]-β-D-glucopyranosyl-(1->4)-1,2-dideoxy-α-D-glucopyrano]-[2,1-d]oxazoline

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