trans-(1R,2R)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:trans-(1R,2R)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene
CAS No.:710314-45-7
Molecular Formula:C₁₈H₁₉NO₄
Molecular Weight:313.353
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-(1R,2R)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

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Technology Process of trans-(1R,2R)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

There total 2 articles about trans-(1R,2R)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

: 710314-45-7
trans-(1R,2R)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

: cis-(1S,2S)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With sodium hydrogencarbonate; In ethanol; for 12h; Inert atmosphere; Reflux;
DOI:10.1002/adsc.201200241

Reference yield:

: 166591-12-4
1,2-dihydro-6,7-dimethoxy-3-nitronaphthalene

: 98-80-6
phenylboronic acid

: 710314-45-7
trans-(1R,2R)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

: cis-(1S,2S)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

Guidance literature:: phenylboronic acid; With (R)-binaphthyldimethylamine phosphoramidite; acetylacetonatobis(ethylene)rhodium(I); In 1,4-dioxane; at 20 ℃; for 0.05h; Inert atmosphere;

1,2-dihydro-6,7-dimethoxy-3-nitronaphthalene; In 1,4-dioxane; water; at 105 ℃; for 20h; Concentration; Reagent/catalyst; enantioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201200241

Reference yield:

: 710314-45-7
trans-(1R,2R)-6,7-dimethoxy-2-nitro-1-phenyl-1,2,3,4-tetrahydronaphthalene

: 406174-91-2
(1R,2R)-6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydronaphthalen-2-ylamine

Guidance literature:: With hydrogenchloride; zinc; In ethanol; at 20 ℃; for 0.333333h; enantioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201200241