C₅₉H₅₈O₁₂

Base Information

• Chemical Name: C₅₉H₅₈O₁₂
• CAS No.: 1402924-06-4
• Molecular Formula: C₅₉H₅₈O₁₂
• Molecular Weight: 959.102
• Mol file: 1402924-06-4.mol

Synonyms:

Chemical Property of C₅₉H₅₈O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₅₈O₁₂

There total 2 articles about C₅₉H₅₈O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C57H54O12 (1402919-94-1) + dimethyl sulfate (77-78-1) → C59H58O12 (1402919-95-2,1402924-05-3,1402924-06-4)

Guidance literature:

C₅₇H₅₄O₁₂; With lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 30h;

dimethyl sulfate; for 16h; Reflux;

DOI:10.1039/c4cc02559h

Reference yield:

32,35,52,55,72,75,92,95-octamethoxy-1,3,5,7,9(1,4)-pentabenzenacyclodecaphane-12,15-diyl bis(trifluoromethanesulfonate) (1402919-93-0) + 4-methoxycarbonylphenylboronic acid (99768-12-4) → C59H58O12 (1402919-95-2,1402924-05-3,1402924-06-4)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; water; at 80 ℃; for 24h;

DOI:10.1021/ja3082523

Reference yield:

C59H58O12 (1402919-95-2,1402924-05-3,1402924-06-4) → C57H54O12 (1402919-94-1)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water; at 50 ℃; for 12h;

DOI:10.1021/ja3082523

upstream raw materials:

3²,3⁵,5²,5⁵,7²,7⁵,9²,9⁵-octamethoxy-1,3,5,7,9(1,4)-pentabenzenacyclodecaphane-1²,1⁵-diyl bis(trifluoromethanesulfonate)

4-methoxycarbonylphenylboronic acid

C₅₇H₅₄O₁₂

dimethyl sulfate

Downstream raw materials:

C₅₇H₅₄O₁₂