Technology Process of C41H63N7O11SSi
There total 16 articles about C41H63N7O11SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: aq. NaOH
2: aq. NaOH / acetone
3: N-methylmorpholine / tetrahydrofuran
5: 1.) NaH / 1.) THF
6: lithium aluminum hydride / tetrahydrofuran / -78 °C
7: NaHSO3 / tetrahydrofuran; H2O
8: ethyl acetate
10: 1 h / 23 °C
With
4-methyl-morpholine; sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; sodium hydrogensulfite;
In
tetrahydrofuran; water; ethyl acetate; acetone;
DOI:10.1016/S0040-4039(00)74237-7
- Guidance literature:
-
Multi-step reaction with 9 steps
1: aq. NaOH / acetone
2: N-methylmorpholine / tetrahydrofuran
4: 1.) NaH / 1.) THF
5: lithium aluminum hydride / tetrahydrofuran / -78 °C
6: NaHSO3 / tetrahydrofuran; H2O
7: ethyl acetate
9: 1 h / 23 °C
With
4-methyl-morpholine; sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; sodium hydrogensulfite;
In
tetrahydrofuran; water; ethyl acetate; acetone;
DOI:10.1016/S0040-4039(00)74237-7
- Guidance literature:
-
Multi-step reaction with 6 steps
2: LiOH / methanol; H2O
3: HCl / diethyl ether; CH2Cl2
4: Ac2O
5: N-methylmorpholine / tetrahydrofuran
6: 1 h / 23 °C
With
4-methyl-morpholine; hydrogenchloride; lithium hydroxide; acetic anhydride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1016/S0040-4039(00)74237-7
