1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

Base Information

Chemical Name:1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol
CAS No.:115262-45-8
Molecular Formula:C₂₅H₃₃NO₅
Molecular Weight:427.541
Hs Code.:

Synonyms:

Suppliers and Price of 1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

Chemical Property:

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Technology Process of 1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

There total 1 articles about 1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(3-benzyloxy-4-methoxyphenacyl)-3-(1,1-ethylenedioxyethyl)pyridinium bromide

: 115262-45-8,115262-74-3
1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

Guidance literature:: With sodium tetrahydroborate; hydrogen; 1.) Adams; Yield given. Multistep reaction; 1.) aq. EtOH (50percent), room temp., 16 h; 2.) aq. NaOH (1N), room temp., 24 h;

Reference yield: 98.0%

: 115262-45-8,115262-74-3
1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

: 115262-46-9,115262-75-4
1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

Guidance literature:: With hydrogenchloride; at 40 ℃; for 2.5h;

Reference yield:

: 115262-45-8,115262-74-3
1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

: 73053-73-3,73650-71-2
(+/-)-trans-1-(3-benzyloxy-4-methoxyphenethyl)-5-ethyl-2-oxo-4-piperidineacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: 98 percent / aq. HCl (1N) / 2.5 h / 40 °C

2: 76 percent / Hg(OAc)2-EDTA / aq. acetic acid / 1.5 h / Heating

3: 71 percent / H₂ / Pd-C (10percent) / ethanol; aq. HClO₄ / 42 h / 35 °C / 2280 - 2850 Torr

4: 84 percent / aq. hydrazine hydrate (80percent), KOH / ethane-1,2-diol / 1.) 120 deg C, 1 h; 2.) 190 deg C, 3.5 h

5: 97 percent / K₂CO₃ / acetone / 30 h / Heating

6: 77 percent / lithium diisopropylamide (LDA), hexamethylphosphoramide (HMPA) / tetrahydrofuran / 2 h / -78 °C

7: 1.17 g / sodium metaperiodate (NaIO₄) / methanol; H₂O / 24 h / Ambient temperature

8: 631 mg / CaCO₃ / toluene / 1 h / Heating

9: 1.) Na-EtOH; 2.) aq. NaOH (1N) / 1.) EtOH, 70 deg C, 2 h, reflux, 6 h; 2.) EtOH, 50 deg C, 4 h

10: 59 percent / aq. AcOH (60percent) / 6 h / Heating

11: 91 percent / HCl / 24 h / Ambient temperature

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; sodium hydroxide; sodium periodate; ethanol; Hg(OAc)2*EDTA; hydrogen; sodium; potassium carbonate; hydrazine hydrate; acetic acid; calcium carbonate; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; perchloric acid; ethanol; water; ethylene glycol; acetic acid; acetone; toluene;