4-thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole

Base Information

Chemical Name:4-thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole
CAS No.:129548-77-2
Molecular Formula:C₃₄H₃₄N₃O₁₂PS
Molecular Weight:739.697
Hs Code.:

4-<diethylphosphono)methyl>thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole

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Technology Process of 4-thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole

There total 3 articles about 4-thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10419-77-9
diethyl iodomethanephosphonate

: 129548-77-2
4-thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / NaOEt / ethanol / 41 h / Heating

2: 1) TMSCl, 2) TMSOTf / 1) HMDS, xylene, 130 deg C, 10 min, 2) MeCN, r.t., 42 min

With chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; sodium ethanolate; In ethanol;
DOI:10.1039/P19900000955

Reference yield:

: 31618-90-3
diethyl (p-toluenesulfonyloxymethane)phosphonate

: 129548-77-2
4-thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / methanol / 11 h / Heating

2: 1) TMSCl, 2) TMSOTf / 1) HMDS, xylene, 130 deg C, 10 min, 2) MeCN, r.t., 42 min

With chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; In methanol;
DOI:10.1039/P19900000955

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 129548-76-1
4(5)-thio-5(4)-nitroimidazole

: 129548-77-2
4-thio-5-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole

: 129548-78-3
5-thio-4-nitro-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)imidazole

Guidance literature:: With chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; Yield given. Multistep reaction. Yields of byproduct given; 1) HMDS, xylene, 130 deg C, 10 min, 2) MeCN, r.t., 42 min;
DOI:10.1039/P19900000955