H-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2*HCl

Base Information

Chemical Name:H-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2*HCl
CAS No.:78841-18-6
Molecular Formula:C₃₄H₄₆ClN₇O₉S*ClH
Molecular Weight:800.761
Hs Code.:

H-Hcy(CH2-CO-Lys<Z(oCl)>-Asn-Phe-OMe)-NH2*HCl

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2*HCl

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Technology Process of H-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2*HCl

There total 5 articles about H-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2*HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78857-65-5
Boc-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2

: 78841-18-6
H-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2*HCl

Guidance literature:: With hydrogenchloride; In acetic acid; for 0.5h; Ambient temperature;

Reference yield:

: 4976-87-8
H-Asn-Phe-OMe*HCl

: 78841-18-6
H-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2*HCl

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / NEt₃ / dimethylformamide / 1.) 30 min, 0 deg C, 2.) 12 h, room temp.

2: aq. HCl / dioxane / 0.5 h / Ambient temperature

3: 92 percent / NEt₃ / dimethylformamide / 1.) 30 min, 0 deg C, 2.) 12 h, room temp.

4: aq. HCl / acetic acid / 0.5 h / Ambient temperature

With hydrogenchloride; triethylamine; In 1,4-dioxane; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 78841-25-5
N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine pentafluorophenyl ester

: 78841-18-6
H-Hcy(CH2-CO-Lys-Asn-Phe-OMe)-NH2*HCl

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / NEt₃ / dimethylformamide / 1.) 30 min, 0 deg C, 2.) 12 h, room temp.

2: aq. HCl / dioxane / 0.5 h / Ambient temperature

3: 92 percent / NEt₃ / dimethylformamide / 1.) 30 min, 0 deg C, 2.) 12 h, room temp.

4: aq. HCl / acetic acid / 0.5 h / Ambient temperature

With hydrogenchloride; triethylamine; In 1,4-dioxane; acetic acid; N,N-dimethyl-formamide;