meso-tetraphenyl-1-<3->porphyrin

Base Information

• Chemical Name: meso-tetraphenyl-1-<3->porphyrin
• CAS No.: 76450-99-2
• Molecular Formula: C₅₆H₄₉N₆O₂
• Molecular Weight: 838.044

Synonyms:

Chemical Property of meso-tetraphenyl-1-<3->porphyrin

Chemical Property:

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Technology Process of meso-tetraphenyl-1-<3->porphyrin

There total 4 articles about meso-tetraphenyl-1-<3->porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

4-amino-2,2,6,6-tetramethyl-1-piperidine-1-oxyl (14691-88-4,78774-22-8) + (Z)-3-((5Z,10Z,14Z,19Z)-5,10,15,20-Tetraphenyl-porphyrin-2-yl)-acryloyl chloride (114658-82-1) → meso-tetraphenyl-1-<3->porphyrin (76450-99-2,76451-00-8) + meso-tetraphenyl-1-<3->porphyrin (76450-99-2,76451-00-8)

Guidance literature:

With pyridine; In tetrahydrofuran; for 3h; Heating;

DOI:10.1021/ja00395a016

Reference yield: 56.0%

4-amino-2,2,6,6-tetramethyl-1-piperidine-1-oxyl (14691-88-4,78774-22-8) + (Z)-3-((5Z,10Z,14Z,19Z)-5,10,15,20-Tetraphenyl-porphyrin-2-yl)-acryloyl chloride (114658-82-1) → meso-tetraphenyl-1-<3->porphyrin (76450-99-2,76451-00-8) + meso-tetraphenyl-1-<3->porphyrin (76450-99-2,76451-00-8)

Guidance literature:

With pyridine; In tetrahydrofuran; for 3h; Heating;

DOI:10.1021/ja00395a016

Reference yield:

meso-tetraphenylporphyrin-1-acrylic acid (69362-71-6,69362-72-7,114658-81-0) → meso-tetraphenyl-1-<3->porphyrin (76450-99-2,76451-00-8)

Guidance literature:

Multi-step reaction with 2 steps

1: oxalyl chloride / benzene / 3 h / Heating

2: 63 percent / pyridine / tetrahydrofuran / 3 h / Heating

With pyridine; oxalyl dichloride; In tetrahydrofuran; benzene;

DOI:10.1021/ja00395a016

upstream raw materials:

4-amino-2,2,6,6-tetramethyl-1-piperidine-1-oxyl

(Z)-3-((5Z,10Z,14Z,19Z)-5,10,15,20-Tetraphenyl-porphyrin-2-yl)-acryloyl chloride

meso-tetraphenylporphyrin-1-acrylic acid

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