9-acetyl-3-chloro-9H-carbazole

Base Information

• Chemical Name: 9-acetyl-3-chloro-9H-carbazole
• CAS No.: 10336-16-0
• Molecular Formula: C14H10ClNO
• Molecular Weight: 243.68800
• Hs Code.: 2933990090
• Mol file: 10336-16-0.mol

Synonyms:9-Acetyl-3-chlor-carbazol;N-Acetyl-3-chlor-carbazol;3-chloro-N-acetylcarbazole;9-acetyl-3-chlorocarbazole;N-acetyl-3-chlorocarbazole;

Chemical Property of 9-acetyl-3-chloro-9H-carbazole

Chemical Property:

• PSA: 22.00000
• LogP: 4.10800

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9-acetyl-3-chloro-9H-carbazole

There total 17 articles about 9-acetyl-3-chloro-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N-(3'-chloro-[1,1'-biphenyl]-2-yl)acetamide (1081540-47-7) → 3-chloro-N-acetylcarbazole (10336-16-0)

Guidance literature:

With sodium persulfate; tetrabutylammomium bromide; In water; for 1.5h; Schlenk technique; Inert atmosphere; Sealed tube; Reflux;

DOI:10.1039/c7gc03130k

Reference yield: 87.0%

N-(5-chloro-[1,1'-biphenyl]-2-yl)acetamide (7148-08-5) → 3-chloro-N-acetylcarbazole (10336-16-0)

Guidance literature:

With sodium persulfate; tetrabutylammomium bromide; In water; for 1.5h; Schlenk technique; Inert atmosphere; Sealed tube; Reflux;

DOI:10.1039/c7gc03130k

Reference yield: 80.0%

3-chlorophenylboronic acid (63503-60-6) + Acetanilid (103-84-4) → 3-chloro-N-acetylcarbazole (10336-16-0)

Guidance literature:

With furan-2-carboxylic acid (phenyl-pyridin-2-yl-methylene)hydrazide; potassium carbonate; In water; at 60 ℃; for 10h; Catalytic behavior; Green chemistry;

DOI:10.1039/c5gc02937f

upstream raw materials:

3-chloro-9H-carbazole

acetic anhydride

vinyl acetate

9-acetylcarbazole