Technology Process of Benzenesulfonic acid 2-(6-methoxy-naphthalen-1-yl)-ethyl ester
There total 4 articles about Benzenesulfonic acid 2-(6-methoxy-naphthalen-1-yl)-ethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 93 percent / lithium aluminum hydride / diethyl ether / Ambient temperature
2: pyridine / 2 h / Ambient temperature
With
pyridine; lithium aluminium tetrahydride;
In
diethyl ether;
DOI:10.1021/jo00350a024
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 10percent Pd/C, 1,1-diphenylethylene, 1-methylnaphthalene / 3 h / 250 - 260 °C
2: 93 percent / lithium aluminum hydride / diethyl ether / Ambient temperature
3: pyridine / 2 h / Ambient temperature
With
pyridine; 1,1-Diphenylethylene; palladium on activated charcoal; lithium aluminium tetrahydride; 1-Methylnaphthalene;
In
diethyl ether;
DOI:10.1021/jo00350a024
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) N-isopropylcyclohexylamine, n-butyllithium / 1.) THF, hexane, -75 deg C, 15 min, 2.) THF, hexane, -78 deg C, 1.5 h
2: 10percent Pd/C, 1,1-diphenylethylene, 1-methylnaphthalene / 3 h / 250 - 260 °C
3: 93 percent / lithium aluminum hydride / diethyl ether / Ambient temperature
4: pyridine / 2 h / Ambient temperature
With
pyridine; 1,1-Diphenylethylene; palladium on activated charcoal; lithium aluminium tetrahydride; n-butyllithium; N-cyclohexylisopropylamine; 1-Methylnaphthalene;
In
diethyl ether;
DOI:10.1021/jo00350a024
