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N,N'-bis(methoxycarbonyl)-2,3-diaza-7-<5'-hydroxy-3,3-dimethyl-2-tetrahydrofuranylidene>bicyclo<2.2.1>heptane

Base Information Edit
  • Chemical Name:N,N'-bis(methoxycarbonyl)-2,3-diaza-7-<5'-hydroxy-3,3-dimethyl-2-tetrahydrofuranylidene>bicyclo<2.2.1>heptane
  • CAS No.:110611-05-7
  • Molecular Formula:C16H24N2O6
  • Molecular Weight:340.376
  • Hs Code.:
  • Mol file:110611-05-7.mol
N,N'-bis(methoxycarbonyl)-2,3-diaza-7-<5'-hydroxy-3,3-dimethyl-2-tetrahydrofuranylidene>bicyclo<2.2.1>heptane

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Chemical Property of N,N'-bis(methoxycarbonyl)-2,3-diaza-7-<5'-hydroxy-3,3-dimethyl-2-tetrahydrofuranylidene>bicyclo<2.2.1>heptane Edit
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Technology Process of N,N'-bis(methoxycarbonyl)-2,3-diaza-7-<5'-hydroxy-3,3-dimethyl-2-tetrahydrofuranylidene>bicyclo<2.2.1>heptane

There total 9 articles about N,N'-bis(methoxycarbonyl)-2,3-diaza-7-<5'-hydroxy-3,3-dimethyl-2-tetrahydrofuranylidene>bicyclo<2.2.1>heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1: 95 percent / diethyl ether / 120 h / 4 °C
2: 96 percent / dipotassium azodicarboxylate, glacial acetic acid / CH2Cl2 / 3 h / 0 °C
3: 95 percent / 70percent aq. acetic acid / 120 h / 55 °C
With potassium diazodicarboxylate; acetic acid; In diethyl ether; dichloromethane;
DOI:10.1021/jo00230a001
Guidance literature:
Multi-step reaction with 2 steps
1: 96 percent / dipotassium azodicarboxylate, glacial acetic acid / CH2Cl2 / 3 h / 0 °C
2: 95 percent / 70percent aq. acetic acid / 120 h / 55 °C
With potassium diazodicarboxylate; acetic acid; In dichloromethane;
DOI:10.1021/jo00230a001
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