Technology Process of C26H23F6N3O3
There total 9 articles about C26H23F6N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: acetic acid / Reflux
2: sodium tetrahydroborate / tetrahydrofuran; methanol
3: triethylsilane; trifluoroacetic acid / dichloromethane
4: water; lithium hydroxide / tetrahydrofuran; methanol
5: dimethylsulfide borane complex / tetrahydrofuran
6: triethylamine / dichloromethane
7: N,N-dimethyl-formamide
8: titanium(IV) isopropylate / tetrahydrofuran
With
titanium(IV) isopropylate; triethylsilane; sodium tetrahydroborate; dimethylsulfide borane complex; water; acetic acid; triethylamine; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
8: Kulinkovich reaction / 8: Kulinkovich reaction;
DOI:10.1016/j.bmcl.2010.12.014
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium tetrahydroborate / tetrahydrofuran; methanol
2: triethylsilane; trifluoroacetic acid / dichloromethane
3: water; lithium hydroxide / tetrahydrofuran; methanol
4: dimethylsulfide borane complex / tetrahydrofuran
5: triethylamine / dichloromethane
6: N,N-dimethyl-formamide
7: titanium(IV) isopropylate / tetrahydrofuran
With
titanium(IV) isopropylate; triethylsilane; sodium tetrahydroborate; dimethylsulfide borane complex; water; triethylamine; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
7: Kulinkovich reaction / 7: Kulinkovich reaction;
DOI:10.1016/j.bmcl.2010.12.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; lithium hydroxide / tetrahydrofuran; methanol
2: dimethylsulfide borane complex / tetrahydrofuran
3: triethylamine / dichloromethane
4: N,N-dimethyl-formamide
5: titanium(IV) isopropylate / tetrahydrofuran
With
titanium(IV) isopropylate; dimethylsulfide borane complex; water; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
5: Kulinkovich reaction / 5: Kulinkovich reaction;
DOI:10.1016/j.bmcl.2010.12.014