Technology Process of C31H42N4O4S
There total 15 articles about C31H42N4O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: pyridine
2: water; lithium hydroxide / 1,4-dioxane; methanol
3: methanol
4: sulfuric acid / water
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
6: manganese(IV) oxide / dichloromethane
7: sodium tris(acetoxy)borohydride / chloroform
With
pyridine; manganese(IV) oxide; sulfuric acid; water; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
1,4-dioxane; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.03.115
- Guidance literature:
-
Multi-step reaction with 3 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
2: manganese(IV) oxide / dichloromethane
3: sodium tris(acetoxy)borohydride / chloroform
With
manganese(IV) oxide; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.03.115
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylsilane; trifluoroacetic acid / dichloromethane
2: palladium 10% on activated carbon; hydrogen / ethyl acetate
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
4: manganese(IV) oxide / dichloromethane
5: sodium tris(acetoxy)borohydride / chloroform
With
triethylsilane; manganese(IV) oxide; palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.03.115