Technology Process of 5-amino-1-imidazole-4-carboxamide
There total 3 articles about 5-amino-1-imidazole-4-carboxamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) HBr / 1) acetic acid, 4 h, reflux; 2) DMF, 2 h, reflux
2: 1.) hydrazine hydrate, 2.) hydrochloric acid / 1) ethanol, reflux, 10 min; 2) ethanol, reflux, 15 min
3: acetonitrile / 0.25 h / Heating
With
hydrogenchloride; hydrogen bromide; hydrazine hydrate;
In
acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) hydrazine hydrate, 2.) hydrochloric acid / 1) ethanol, reflux, 10 min; 2) ethanol, reflux, 15 min
2: acetonitrile / 0.25 h / Heating
With
hydrogenchloride; hydrazine hydrate;
In
acetonitrile;
- Guidance literature:
-
In
acetonitrile;
for 0.25h;
Yield given;
Heating;
