2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone

Base Information

Chemical Name:2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone
CAS No.:129207-79-0
Molecular Formula:C₁₈H₂₀O₈
Molecular Weight:364.352
Hs Code.:

Synonyms:

Suppliers and Price of 2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone

There total 7 articles about 2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 129207-79-0
2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone

Guidance literature:: Multi-step reaction with 7 steps

1: pyridinium chlorochromate / CH₂Cl₂ / 3 h

2: sodium acetate / acetic anhydride / Heating

3: NaOH / H₂O / Heating

4: hydroxylamine hydrochloride / aq. NaOH / 0.5 h / 60 °C

5: acetic anhydride / 0.08 h / Heating

6: ZnCl₂, HCl / diethyl ether / 5 h / 0 °C

7: 2.0 g / aq. potassium persulphate / aq. KOH / Ambient temperature

With hydrogenchloride; sodium hydroxide; potassium peroxomonosulphate; hydroxylamine hydrochloride; sodium acetate; acetic anhydride; pyridinium chlorochromate; zinc(II) chloride; In potassium hydroxide; sodium hydroxide; diethyl ether; dichloromethane; water; acetic anhydride;

Reference yield:

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 129207-79-0
2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone

Guidance literature:: Multi-step reaction with 8 steps

1: lithium aluminium hydride / diethyl ether / 3 h / Heating

2: pyridinium chlorochromate / CH₂Cl₂ / 3 h

3: sodium acetate / acetic anhydride / Heating

4: NaOH / H₂O / Heating

5: hydroxylamine hydrochloride / aq. NaOH / 0.5 h / 60 °C

6: acetic anhydride / 0.08 h / Heating

7: ZnCl₂, HCl / diethyl ether / 5 h / 0 °C

8: 2.0 g / aq. potassium persulphate / aq. KOH / Ambient temperature

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; potassium peroxomonosulphate; hydroxylamine hydrochloride; sodium acetate; acetic anhydride; pyridinium chlorochromate; zinc(II) chloride; In potassium hydroxide; sodium hydroxide; diethyl ether; dichloromethane; water; acetic anhydride;

Reference yield:

: 13338-63-1
2-(3,4,5-trimethoxyphenyl)acetonitrile

: 129207-79-0
2,4,5-Trihydroxy-6-methoxyphenyl-3,4,5-trimethoxybenzyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: ZnCl₂, HCl / diethyl ether / 5 h / 0 °C

2: 2.0 g / aq. potassium persulphate / aq. KOH / Ambient temperature

With hydrogenchloride; potassium peroxomonosulphate; zinc(II) chloride; In potassium hydroxide; diethyl ether;