Technology Process of C12H13NO4
There total 6 articles about C12H13NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / dimethyl sulfoxide / 5 h / 20 °C
2: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C
3: dichloromethane / 3 h / -10 - 25 °C / Inert atmosphere
4: 120 h / 20 °C / Inert atmosphere
With
pyridinium chlorochromate; potassium hydroxide;
In
dichloromethane; dimethyl sulfoxide;
3: Wittig reaction;
DOI:10.1515/HC.2011.043
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C
2: dichloromethane / 3 h / -10 - 25 °C / Inert atmosphere
3: 120 h / 20 °C / Inert atmosphere
With
pyridinium chlorochromate;
In
dichloromethane;
2: Wittig reaction;
DOI:10.1515/HC.2011.043
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide / dimethyl sulfoxide / 5 h / 20 °C
2: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C
3: dichloromethane / 3 h / -10 - 25 °C / Inert atmosphere
With
pyridinium chlorochromate; potassium hydroxide;
In
dichloromethane; dimethyl sulfoxide;
3: Wittig reaction;
DOI:10.1515/HC.2011.043
