N,N'-Bis-(4-phenylbutyl)-azulene-1,3-dimethanamine di-hydrogenoxalate

Base Information

Chemical Name:N,N'-Bis-(4-phenylbutyl)-azulene-1,3-dimethanamine di-hydrogenoxalate
CAS No.:141914-71-8
Molecular Formula:2C₂H₂O₄*C₃₂H₃₈N₂
Molecular Weight:630.738
Hs Code.:

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Chemical Property of N,N'-Bis-(4-phenylbutyl)-azulene-1,3-dimethanamine di-hydrogenoxalate

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Technology Process of N,N'-Bis-(4-phenylbutyl)-azulene-1,3-dimethanamine di-hydrogenoxalate

There total 3 articles about N,N'-Bis-(4-phenylbutyl)-azulene-1,3-dimethanamine di-hydrogenoxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4-Phenyl-butyl)-[1-(3-{[(Z)-4-phenyl-butylimino]-methyl}-azulen-1-yl)-meth-(Z)-ylidene]-amine

: 141914-71-8
N,N'-Bis-(4-phenylbutyl)-azulene-1,3-dimethanamine di-hydrogenoxalate

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 5h; Yield given; Heating;
DOI:10.1002/ardp.19923250408

Reference yield:

: 13214-66-9
4-phenyl-1-butylamine

: 141914-71-8
N,N'-Bis-(4-phenylbutyl)-azulene-1,3-dimethanamine di-hydrogenoxalate

Guidance literature:: Multi-step reaction with 2 steps

1: p-TsOH / CHCl₃ / Heating

2: NaBH₄ / ethanol / 5 h / Heating

With sodium tetrahydroborate; toluene-4-sulfonic acid; In ethanol; chloroform;
DOI:10.1002/ardp.19923250408

Reference yield:

: 38337-21-2
azulene-1,3-dicarbaldehyde

: 141914-71-8
N,N'-Bis-(4-phenylbutyl)-azulene-1,3-dimethanamine di-hydrogenoxalate

Guidance literature:: Multi-step reaction with 2 steps

1: p-TsOH / CHCl₃ / Heating

2: NaBH₄ / ethanol / 5 h / Heating

With sodium tetrahydroborate; toluene-4-sulfonic acid; In ethanol; chloroform;
DOI:10.1002/ardp.19923250408