benzyl (2R,5R,6R)-(Z)-(3-β-hydroxyethylidene)-6-(1-hydroxypropyl)-7-methoxycarbonyl-(Z)-methylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate

Base Information

• Chemical Name: benzyl (2R,5R,6R)-(Z)-(3-β-hydroxyethylidene)-6-(1-hydroxypropyl)-7-methoxycarbonyl-(Z)-methylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate
• CAS No.: 85339-65-7
• Molecular Formula: C₂₁H₂₅NO₇
• Molecular Weight: 403.432

Synonyms:

Chemical Property of benzyl (2R,5R,6R)-(Z)-(3-β-hydroxyethylidene)-6-(1-hydroxypropyl)-7-methoxycarbonyl-(Z)-methylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of benzyl (2R,5R,6R)-(Z)-(3-β-hydroxyethylidene)-6-(1-hydroxypropyl)-7-methoxycarbonyl-(Z)-methylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate

There total 2 articles about benzyl (2R,5R,6R)-(Z)-(3-β-hydroxyethylidene)-6-(1-hydroxypropyl)-7-methoxycarbonyl-(Z)-methylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

→ benzyl (2R,5R,6R)-(Z)-(3-β-hydroxyethylidene)-6-(1-hydroxypropyl)-7-methoxycarbonyl-(Z)-methylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate (85339-65-7,112711-42-9,112711-43-0)

Guidance literature:

Reference yield: 7.0%

propionaldehyde (123-38-6) + benzyl (2R,5R)-(Z)-3-(β-hydroxyethylidene)-(Z)-7-methoxycarbonylmethylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate (80282-00-4) → benzyl (2R,5R,6R)-(Z)-(3-β-hydroxyethylidene)-6-(1-hydroxypropyl)-7-methoxycarbonyl-(Z)-methylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate (85339-65-7,112711-42-9,112711-43-0) + benzyl (2R,5R)-(Z)-(3-β-hydroxyethylidene)-7-methoxycarbonyl-(E)-methylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate (80300-67-0)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 2h;

upstream raw materials:

propionaldehyde

benzyl (2R,5R)-(Z)-3-(β-hydroxyethylidene)-(Z)-7-methoxycarbonylmethylene-4-oxa-1-azabicyclo<3.2.0>heptane-2-carboxylate

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