C₁₉H₃₀ClNO₃Si

Base Information Edit

Chemical Name:C₁₉H₃₀ClNO₃Si
CAS No.:1380210-51-4
Molecular Formula:C₁₉H₃₀ClNO₃Si
Molecular Weight:383.991
Hs Code.:
Mol file:1380210-51-4.mol

C<sub>19</sub>H<sub>30</sub>ClNO<sub>3</sub>Si

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Chemical Property of C₁₉H₃₀ClNO₃Si Edit

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Technology Process of C₁₉H₃₀ClNO₃Si

There total 4 articles about C₁₉H₃₀ClNO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380210-47-8
(S,E)-N-[1-(tert-butyldimethylsilyloxy)-6-chloro-3-oxohex-4-en-2-yl]benzamide

: 1380210-55-8
C₁₉H₃₀ClNO₃Si

: 1380210-51-4
C₁₉H₃₀ClNO₃Si

Guidance literature:: With lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; ethanol; at -78 ℃; for 4h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201200064

Reference yield:

: 933468-31-6
N-benzoyl-O-((tert-butyl)-dimethylsilyl)-(S)-serine methyl ester

: 1380210-51-4
C₁₉H₃₀ClNO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylaluminum / hexane; dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: methyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran; ethanol / 4 h / -78 °C / Inert atmosphere

With methyllithium; trimethylaluminum; lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; ethanol; hexane; dichloromethane;
DOI:10.1002/ejoc.201200064

Reference yield:

: 933468-32-7
C₁₈H₃₀N₂O₄Si

: 1380210-51-4
C₁₉H₃₀ClNO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: methyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran; ethanol / 4 h / -78 °C / Inert atmosphere

With methyllithium; lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; ethanol; hexane;
DOI:10.1002/ejoc.201200064