N2-[(9H-Fluoren-9-ylmethoxy)carbonyl]-N-(triphenylmethyl)-L-asparagine 2,4,5-trichlorophenyl ester

Base Information

Chemical Name:N2-[(9H-Fluoren-9-ylmethoxy)carbonyl]-N-(triphenylmethyl)-L-asparagine 2,4,5-trichlorophenyl ester
CAS No.:132388-62-6
Molecular Formula:C₄₄H₃₃Cl₃N₂O₅
Molecular Weight:776.115
Hs Code.:
DSSTox Substance ID:DTXSID501115069

Synonyms:DTXSID501115069;132388-62-6;N2-[(9H-Fluoren-9-ylmethoxy)carbonyl]-N-(triphenylmethyl)-L-asparagine 2,4,5-trichlorophenyl ester

Suppliers and Price of N2-[(9H-Fluoren-9-ylmethoxy)carbonyl]-N-(triphenylmethyl)-L-asparagine 2,4,5-trichlorophenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N2-[(9H-Fluoren-9-ylmethoxy)carbonyl]-N-(triphenylmethyl)-L-asparagine 2,4,5-trichlorophenyl ester

Chemical Property:

XLogP3:10.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:13
Exact Mass:774.145505
Heavy Atom Count:54
Complexity:1180

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(C2=CC=CC=C2)(C3=CC=CC=C3)NC(=O)CC(C(=O)OC4=CC(=C(C=C4Cl)Cl)Cl)NC(=O)OCC5C6=CC=CC=C6C7=CC=CC=C57
Isomeric SMILES:C1=CC=C(C=C1)C(C2=CC=CC=C2)(C3=CC=CC=C3)NC(=O)C[C@@H](C(=O)OC4=CC(=C(C=C4Cl)Cl)Cl)NC(=O)OCC5C6=CC=CC=C6C7=CC=CC=C57

Technology Process of N2-[(9H-Fluoren-9-ylmethoxy)carbonyl]-N-(triphenylmethyl)-L-asparagine 2,4,5-trichlorophenyl ester

There total 4 articles about N2-[(9H-Fluoren-9-ylmethoxy)carbonyl]-N-(triphenylmethyl)-L-asparagine 2,4,5-trichlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 132388-62-6
Fmoc-Asn(trityl) 2,4,5-trichlorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / acetic anhydride, conc.H₂SO₄ / acetic acid / 1.25 h / 60 °C

3: DCC

With sulfuric acid; acetic anhydride; dicyclohexyl-carbodiimide; In acetic acid;
DOI:10.1016/S0040-4039(00)74872-6

Reference yield:

: 132388-57-9
N-benzyloxycarbonyl-N'-trityl-L-asparagine

: 132388-62-6
Fmoc-Asn(trityl) 2,4,5-trichlorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd-C

3: DCC

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal;
DOI:10.1016/S0040-4039(00)74872-6