Benzamide, N,N'-1,2-phenylenebis[2-hydroxy-

Base Information

Chemical Name:Benzamide, N,N'-1,2-phenylenebis[2-hydroxy-
CAS No.:103528-00-3
Molecular Formula:C20H16N2O4
Molecular Weight:348.358
Hs Code.:
DSSTox Substance ID:DTXSID00477137
Nikkaji Number:J169.227E
Wikidata:Q82309374
Mol file:103528-00-3.mol

Synonyms:Benzamide, N,N'-1,2-phenylenebis[2-hydroxy-;103528-00-3;SCHEMBL7678596;DTXSID00477137;1,2-bis-(2-hydroxybenzamido)benzene

Suppliers and Price of Benzamide, N,N'-1,2-phenylenebis[2-hydroxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzamide, N,N'-1,2-phenylenebis[2-hydroxy-

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:348.11100700
Heavy Atom Count:26
Complexity:454

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)NC2=CC=CC=C2NC(=O)C3=CC=CC=C3O)O

Technology Process of Benzamide, N,N'-1,2-phenylenebis[2-hydroxy-

There total 4 articles about Benzamide, N,N'-1,2-phenylenebis[2-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 95-54-5
1,2-diamino-benzene

: 1441-87-8
salicyloyl chloride

: 103528-00-3
N,N’-(1,2-phenylene)bis(2-hydroxybenzamide)

Guidance literature:: at 100 ℃; for 0.166667h;
DOI:10.1055/s-1993-25893

Reference yield: 77.0%

: 75-52-5
nitromethane

: 41350-19-0
1,2-bis(2-acetoxybenzamido)benzene

: 103528-00-3
N,N’-(1,2-phenylene)bis(2-hydroxybenzamide)

Guidance literature:: 1,2-bis(2-acetoxybenzamido)benzene; With sodium hydroxide; In water; acetone; at 20 ℃; Inert atmosphere; Schlenk technique;

With hydrogenchloride; In water; acetone; at 0 ℃; Inert atmosphere; Schlenk technique;

nitromethane;
DOI:10.1021/acs.inorgchem.5b00159

Reference yield: 72.0%

: 95-54-5
1,2-diamino-benzene

: 5538-51-2
O-acetylsalicyloyl chloride

: 103528-00-3
N,N’-(1,2-phenylene)bis(2-hydroxybenzamide)

Guidance literature:: 1,2-diamino-benzene; O-acetylsalicyloyl chloride; With triethylamine; In dichloromethane; at 30 ℃; for 18h;

With hydrogenchloride; In ethanol; for 10h; Heating;
DOI:10.1021/jacs.5b13337