N-acryl-N-allyl-2-tert-butylanilide

Base Information

Chemical Name:N-acryl-N-allyl-2-tert-butylanilide
CAS No.:193410-54-7
Molecular Formula:C₁₆H₂₁NO
Molecular Weight:243.349
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-acryl-N-allyl-2-tert-butylanilide

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Technology Process of N-acryl-N-allyl-2-tert-butylanilide

There total 10 articles about N-acryl-N-allyl-2-tert-butylanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: allyl-(2-tert-butyl-phenyl)-amine

: 193410-54-7,193410-55-8
N-acryl-N-allyl-2-tert-butylanilide

Guidance literature:: Multi-step reaction with 8 steps

1: tetrahydrofuran

2: LiOH / tetrahydrofuran

3: 85 percent / SOCl₂

4: 70 percent / tetrahydrofuran

5: NaBH₄

8: H₂O₂

With lithium hydroxide; sodium tetrahydroborate; thionyl chloride; dihydrogen peroxide; In tetrahydrofuran; 1: Acylation / 2: Hydrolysis / 3: Esterification / 4: Grignard reaction / 5: Reduction / 6: Acylation / 7: Substitution / 8: Elimination;
DOI:10.1016/S0040-4039(99)01853-5

Reference yield:

: (S,R)-N-allyl-N-2-(tert-butyl)phenyl 2-hydroxypropanamide

: 193410-54-7,193410-55-8
N-acryl-N-allyl-2-tert-butylanilide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / Ambient temperature

2: 1.) PhSeNa, 2.) H₂O₂ / 1.) ethanol, 2.) ethanol, THF, water

With dihydrogen peroxide; sodium phenylselenide; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo9721711

Reference yield:

: (R_a, 2S)-N-allyl-(2-tert-butylphenyl)-2-acetoxypropionamide

: 193410-54-7,193410-55-8
N-acryl-N-allyl-2-tert-butylanilide

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / ethanol / Ambient temperature

2: triethylamine / tetrahydrofuran / Ambient temperature

3: 1.) PhSeNa, 2.) H₂O₂ / 1.) ethanol, 2.) ethanol, THF, water

With sodium hydroxide; dihydrogen peroxide; sodium phenylselenide; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1021/jo9721711