Technology Process of trans-2,3-epoxy-1,4-diphenyl-4-pentene-1-one
There total 5 articles about trans-2,3-epoxy-1,4-diphenyl-4-pentene-1-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride;
In
dichloromethane;
for 48h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / CH2Cl2 / 24 h / Ambient temperature
2: 90 percent / 30 percent H2O2, 6 N NaOH / methanol / 0 - 10 °C
3: 72 percent / 35 percent NaOH, triethylbenzylammonium chloride / CH2Cl2 / 48 h / Ambient temperature
With
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92 percent / MoO5*H2O*HMPA / CH2Cl2 / 168 h / Ambient temperature
2: 47 percent / methyltriphenylphosphonium iodide, triethylbenzylammonium chloride, 35 percent NaOH / CH2Cl2 / 72 h
3: 72 percent / 35 percent NaOH, triethylbenzylammonium chloride / CH2Cl2 / 48 h / Ambient temperature
With
sodium hydroxide; molybdenum peroxide hexamethylphosphorylamide; N-benzyl-N,N,N-triethylammonium chloride; methyl-triphenylphosphonium iodide;
In
dichloromethane;
