C₁₆H₂₇⁽²⁾HO₆Si

Base Information

Chemical Name:C₁₆H₂₇⁽²⁾HO₆Si
CAS No.:91758-44-0
Molecular Formula:C₁₆H₂₈O₆Si
Molecular Weight:345.472
Hs Code.:

C<sub>16</sub>H<sub>27</sub><sup>(2)</sup>HO<sub>6</sub>Si

Synonyms:

Suppliers and Price of C₁₆H₂₇⁽²⁾HO₆Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₆H₂₇⁽²⁾HO₆Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₆H₂₇⁽²⁾HO₆Si

There total 8 articles about C₁₆H₂₇⁽²⁾HO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138-59-0
shikimic acid

: 91758-44-0
C₁₆H₂₇⁽²⁾HO₆Si

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / methanol; diethyl ether / 15 h / Ambient temperature

2: 90 percent / p-toluenesulfonic acid, Na₂CO₃ / CH₂Cl₂ / 5 °C

3: imidazole / dimethylformamide / 1.75 h

4: 1.) H₂O, AcOH; 2) pyridinium dichromate / 1.) methanol, toluene r.t., 1 h; 2.) DMF, 45 deg C, 1 h

5: 1.) CrO₃ in H₂SO₄; 2.) sodium borodeuteride / 1.) acetone, r.t., 3.5 h; 2.) ethanol, 15 min

With 1H-imidazole; dipyridinium dichromate; Jones’ reagent; sodium borodeuteride; water; sodium carbonate; toluene-4-sulfonic acid; acetic acid; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 40983-58-2
methyl shikimate

: 91758-44-0
C₁₆H₂₇⁽²⁾HO₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / p-toluenesulfonic acid, Na₂CO₃ / CH₂Cl₂ / 5 °C

2: imidazole / dimethylformamide / 1.75 h

3: 1.) H₂O, AcOH; 2) pyridinium dichromate / 1.) methanol, toluene r.t., 1 h; 2.) DMF, 45 deg C, 1 h

4: 1.) CrO₃ in H₂SO₄; 2.) sodium borodeuteride / 1.) acetone, r.t., 3.5 h; 2.) ethanol, 15 min

With 1H-imidazole; dipyridinium dichromate; Jones’ reagent; sodium borodeuteride; water; sodium carbonate; toluene-4-sulfonic acid; acetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 88400-31-1
(3aR,7R,7aS)-7-Hydroxy-2-methoxy-2-methyl-3a,6,7,7a-tetrahydro-benzo[1,3]dioxole-5-carboxylic acid methyl ester

: 91758-44-0
C₁₆H₂₇⁽²⁾HO₆Si

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 1.75 h

2: 1.) H₂O, AcOH; 2) pyridinium dichromate / 1.) methanol, toluene r.t., 1 h; 2.) DMF, 45 deg C, 1 h

3: 1.) CrO₃ in H₂SO₄; 2.) sodium borodeuteride / 1.) acetone, r.t., 3.5 h; 2.) ethanol, 15 min

With 1H-imidazole; dipyridinium dichromate; Jones’ reagent; sodium borodeuteride; water; acetic acid; In N,N-dimethyl-formamide;