N-benzyl-2--5-thioxoproline methyl ester

Base Information

Chemical Name:N-benzyl-2--5-thioxoproline methyl ester
CAS No.:139483-90-2
Molecular Formula:C₂₄H₂₇NO₄S
Molecular Weight:425.549
Hs Code.:

N-benzyl-2-<ethyldihydrocinnamoyl>-5-thioxoproline methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-2--5-thioxoproline methyl ester

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Technology Process of N-benzyl-2--5-thioxoproline methyl ester

There total 2 articles about N-benzyl-2--5-thioxoproline methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103301-78-6
1-benzyl-5-oxo-pyrrolidine-2-carboxylic acid methyl ester

: 139483-90-2
N-benzyl-2--5-thioxoproline methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Lawesson's reagent / tetrahydrofuran / 4 h / Ambient temperature

2: 1.) HMDS, n-BuLi / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 3 h

With Lawessons reagent; n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran;

Reference yield:

: 103-36-6
ethyl 3-phenyl-2-propenoate

: 130516-24-4
(S)-(+)-1-Benzyl-5-thioxoproline methyl ester

: 139483-90-2
N-benzyl-2--5-thioxoproline methyl ester

Guidance literature:: With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 3 h;