C₁₄H₁₆N₄O₂S

Base Information

• Chemical Name: C₁₄H₁₆N₄O₂S
• CAS No.: 479500-86-2
• Molecular Formula: C₁₄H₁₆N₄O₂S
• Molecular Weight: 304.373
• Mol file: 479500-86-2.mol

Synonyms:

Chemical Property of C₁₄H₁₆N₄O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₆N₄O₂S

There total 5 articles about C₁₄H₁₆N₄O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzyl-2-mercapto-5-hydroxymethyl-imidazole (98412-23-8) → C14H16N4O2S (479500-86-2)

Guidance literature:

Multi-step reaction with 6 steps

1: 72 percent / NaOH / methanol; H₂O / 20 °C

2: 90 percent / MnO₂ / CHCl₃ / Heating

3: 91 percent / AgNO₃; NaOH / H₂O

4: 81 percent / concentrated sulfuric acid / Heating

5: 95 percent / hydrazine hydrate / ethanol / 0.5 h

6: 95 percent / Heating

With manganese(IV) oxide; sodium hydroxide; sulfuric acid; hydrazine hydrate; silver nitrate; In methanol; ethanol; chloroform; water;

DOI:10.1002/jhet.5570390434

Reference yield:

1-benzyl-2-(ethylsulfanyl)imidazole-5-carbaldehyde (479400-31-2) → C14H16N4O2S (479500-86-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 91 percent / AgNO₃; NaOH / H₂O

2: 81 percent / concentrated sulfuric acid / Heating

3: 95 percent / hydrazine hydrate / ethanol / 0.5 h

4: 95 percent / Heating

With sodium hydroxide; sulfuric acid; hydrazine hydrate; silver nitrate; In ethanol; water;

DOI:10.1002/jhet.5570390434

Reference yield:

2-ethylthio-5-hydroxymethyl-1-phenylmethylimidazole (479400-29-8) → C14H16N4O2S (479500-86-2)

Guidance literature:

Multi-step reaction with 5 steps

1: 90 percent / MnO₂ / CHCl₃ / Heating

2: 91 percent / AgNO₃; NaOH / H₂O

3: 81 percent / concentrated sulfuric acid / Heating

4: 95 percent / hydrazine hydrate / ethanol / 0.5 h

5: 95 percent / Heating

With manganese(IV) oxide; sodium hydroxide; sulfuric acid; hydrazine hydrate; silver nitrate; In ethanol; chloroform; water;

DOI:10.1002/jhet.5570390434

upstream raw materials:

1-benzyl-2-mercapto-5-hydroxymethyl-imidazole

1-benzyl-2-(ethylsulfanyl)imidazole-5-carbaldehyde

2-ethylthio-5-hydroxymethyl-1-phenylmethylimidazole

1-benzyl-2-ethylsulfanylimidazole-5-carboxylic acid methyl ester