C₃₀H₃₄O₃Si

Base Information

Chemical Name:C₃₀H₃₄O₃Si
CAS No.:945979-89-5
Molecular Formula:C₃₀H₃₄O₃Si
Molecular Weight:470.684
Hs Code.:

C<sub>30</sub>H<sub>34</sub>O<sub>3</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₄O₃Si

Chemical Property:

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Technology Process of C₃₀H₃₄O₃Si

There total 12 articles about C₃₀H₃₄O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945979-88-4
C₃₀H₃₆O₃Si

: 945979-89-5
C₃₀H₃₄O₃Si

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; for 4h;
DOI:10.1016/j.tet.2007.05.034

Reference yield:

: 945979-78-2
C₃₇H₅₂O₃Si₂

: 945979-89-5
C₃₀H₃₄O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1: 47 percent / second-generation Grubbs catalyst / CH₂Cl₂ / 15 h / 20 °C

2: 91 percent / TsOH*2H₂O / tetrahydrofuran; H₂O / 24 h / 20 °C

3: IBX / tetrahydrofuran; dimethylsulfoxide / 4 h / 20 °C

4: 324 mg / diethyl ether / 0 - 20 °C

5: IBX / tetrahydrofuran; dimethylsulfoxide / 4 h / 20 °C

With toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/j.tet.2007.05.034

Reference yield:

: 945979-80-6
2-(2,5-dimethoxy-4-methylphenyl)propanal

: 945979-89-5
C₃₀H₃₄O₃Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / 0 - 20 °C

1.2: 87 percent / tetrahydrofuran; hexane / 0 - 20 °C

2.1: 98 percent / CAN / acetonitrile; H₂O / 0.08 h / 20 °C

3.1: 97 percent / Na₂S₂O₄ / diethyl ether; H₂O / 0.58 h / 20 °C

4.1: 73 percent / imidazole; DMAP / CH₂Cl₂ / 0 °C

5.1: 71 percent / DIAD; PPh₃ / tetrahydrofuran / 0 - 20 °C

6.1: 47 percent / second-generation Grubbs catalyst / CH₂Cl₂ / 15 h / 20 °C

7.1: 91 percent / TsOH*2H₂O / tetrahydrofuran; H₂O / 24 h / 20 °C

8.1: IBX / tetrahydrofuran; dimethylsulfoxide / 4 h / 20 °C

9.1: 324 mg / diethyl ether / 0 - 20 °C

10.1: IBX / tetrahydrofuran; dimethylsulfoxide / 4 h / 20 °C

With 1H-imidazole; dmap; n-butyllithium; sodium dithionite; ammonium cerium(IV) nitrate; di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; triphenylphosphine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; acetonitrile; 1.2: Wittig reaction / 5.1: Mitsunobu reaction;
DOI:10.1016/j.tet.2007.05.034