C₅₃H₆₅N₁₃O₁₄

Base Information

Chemical Name:C₅₃H₆₅N₁₃O₁₄
CAS No.:84993-67-9
Molecular Formula:C₅₃H₆₅N₁₃O₁₄
Molecular Weight:1108.18
Hs Code.:

C<sub>53</sub>H<sub>65</sub>N<sub>13</sub>O<sub>14</sub>

Synonyms:

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Chemical Property of C₅₃H₆₅N₁₃O₁₄

Chemical Property:

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Technology Process of C₅₃H₆₅N₁₃O₁₄

There total 20 articles about C₅₃H₆₅N₁₃O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84979-63-5
Z-Arg(NO₂)-Lys(Z)-Asp(OBzl)-Val-Tyr-NHNH₂

: 84993-67-9
C₅₃H₆₅N₁₃O₁₄

Guidance literature:: With hydrogenchloride; isopentyl nitrite; In 1,4-dioxane; at -60 ℃;
DOI:10.1248/cpb.30.3271

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 84993-67-9
C₅₃H₆₅N₁₃O₁₄

Guidance literature:: Multi-step reaction with 10 steps

1: 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide, N-methylmorpholine / dimethylformamide / 0 °C

2: N-methylmorpholine / dimethylformamide / 0 °C

3: trifluoroacetic acid, anisol / 0.33 h / Ambient temperature

4: N-methylmorpholine / dimethylformamide / 0 °C

5: trifluoroacetic acid, anisol / 0.33 h / Ambient temperature

6: N-methylmorpholine / dimethylformamide / 0 °C

7: trifluoroacetic acid, anisol / 0.33 h / Ambient temperature

8: N-methylmorpholine / dimethylformamide / 16 h / 4 °C

9: 79 percent / Zn / acetic acid; dimethylformamide / 3 h / Ambient temperature

10: isoamylnitrite, HCl / dioxane / -60 °C

With 4-methyl-morpholine; hydrogenchloride; methoxybenzene; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; zinc; isopentyl nitrite; In 1,4-dioxane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.30.3271

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 84993-67-9
C₅₃H₆₅N₁₃O₁₄

Guidance literature:: Multi-step reaction with 8 steps

1: 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide, N-methylmorpholine / dimethylformamide / 0 °C

2: N-methylmorpholine / dimethylformamide / 0 °C

3: trifluoroacetic acid, anisol / 0.33 h / Ambient temperature

4: N-methylmorpholine / dimethylformamide / 0 °C

5: trifluoroacetic acid, anisol / 0.33 h / Ambient temperature

6: N-methylmorpholine / dimethylformamide / 16 h / 4 °C

7: 79 percent / Zn / acetic acid; dimethylformamide / 3 h / Ambient temperature

8: isoamylnitrite, HCl / dioxane / -60 °C

With 4-methyl-morpholine; hydrogenchloride; methoxybenzene; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; zinc; isopentyl nitrite; In 1,4-dioxane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.30.3271