Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester

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Chemical Name:Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester
CAS No.:81036-26-2
Molecular Formula:C₂₄H₃₇N₃O₆S₃Si
Molecular Weight:587.858
Hs Code.:

Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester

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Chemical Property of Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester

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Technology Process of Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester

There total 6 articles about Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63216-42-2
γ-<<(p-nitrobenzyl)oxycarbonyl>amino>butyric acid

: 81036-26-2
Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / tetrahydrofuran

2: NaBH₄

5: sodium methylate / methanol / 0.33 h / 0 °C

6: methanol / 0.33 h / 0 °C

With sodium tetrahydroborate; sodium methylate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1248/cpb.29.3158

Reference yield:

: 81036-23-9
(4-Hydroxy-butyl)-carbamic acid 4-nitro-benzyl ester

: 81036-26-2
Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

3: sodium methylate / methanol / 0.33 h / 0 °C

4: methanol / 0.33 h / 0 °C

With sodium methylate; In methanol;
DOI:10.1248/cpb.29.3158

Reference yield:

: 81036-24-0
Methanesulfonic acid 4-(4-nitro-benzyloxycarbonylamino)-butyl ester

: 81036-26-2
Trithiocarbonic acid (2R,3S)-3-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-oxo-azetidin-2-yl ester 4-(4-nitro-benzyloxycarbonylamino)-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: sodium methylate / methanol / 0.33 h / 0 °C

3: methanol / 0.33 h / 0 °C

With sodium methylate; In methanol;
DOI:10.1248/cpb.29.3158