2-Phenyl-2-(4-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3,5,13⁽¹⁷⁾,14,18-hexaen-2-yl-phenyl)-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3⁽¹⁹⁾,4,6⁽¹⁸⁾,13⁽¹⁷⁾,14-hexaene

Base Information

• Chemical Name: 2-Phenyl-2-(4-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3,5,13⁽¹⁷⁾,14,18-hexaen-2-yl-phenyl)-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3⁽¹⁹⁾,4,6⁽¹⁸⁾,13⁽¹⁷⁾,14-hexaene
• CAS No.: 82313-80-2
• Molecular Formula: C₅₀H₅₀
• Molecular Weight: 650.947

Synonyms:

Chemical Property of 2-Phenyl-2-(4-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3,5,13⁽¹⁷⁾,14,18-hexaen-2-yl-phenyl)-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3⁽¹⁹⁾,4,6⁽¹⁸⁾,13⁽¹⁷⁾,14-hexaene

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Technology Process of 2-Phenyl-2-(4-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3,5,13⁽¹⁷⁾,14,18-hexaen-2-yl-phenyl)-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3⁽¹⁹⁾,4,6⁽¹⁸⁾,13⁽¹⁷⁾,14-hexaene

There total 2 articles about 2-Phenyl-2-(4-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3,5,13⁽¹⁷⁾,14,18-hexaen-2-yl-phenyl)-tricyclo[11.2.2.2^3,6]nonadeca-1⁽¹⁶⁾,3⁽¹⁹⁾,4,6⁽¹⁸⁾,13⁽¹⁷⁾,14-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

13-Phenyl<1.6>paracyclophan (82313-64-2) → 2-Phenyl-2-(4-tricyclo[11.2.2.23,6]nonadeca-1(16),3,5,13(17),14,18-hexaen-2-yl-phenyl)-tricyclo[11.2.2.23,6]nonadeca-1(16),3(19),4,6(18),13(17),14-hexaene (82313-80-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 47 percent / Br₂ / CCl₄ / 30 °C / Irradiation

2: CrCl₂ / dimethylformamide / Ambient temperature

With chromium dichloride; bromine; In tetrachloromethane; N,N-dimethyl-formamide;

Reference yield:

13-Brom-13-phenyl<1.6>paracyclophan (82272-80-8) → 2-Phenyl-2-(4-tricyclo[11.2.2.23,6]nonadeca-1(16),3,5,13(17),14,18-hexaen-2-yl-phenyl)-tricyclo[11.2.2.23,6]nonadeca-1(16),3(19),4,6(18),13(17),14-hexaene (82313-80-2) + 2-Phenyl-2-(4-tricyclo[11.2.2.23,6]nonadeca-1(16),3(19),4,6(18),13(17),14-hexaen-2-ylidene-cyclohexa-2,5-dienyl)-tricyclo[11.2.2.23,6]nonadeca-1(16),3(19),4,6(18),13(17),14-hexaene

Guidance literature:

With chromium dichloride; In N,N-dimethyl-formamide; Yield given; Ambient temperature;

upstream raw materials:

13-Brom-13-phenyl<1.6>paracyclophan

13-Phenyl<1.6>paracyclophan

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