[((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl₂]

Base Information

Chemical Name:[((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl₂]
CAS No.:81191-75-5
Molecular Formula:C₃₇H₃₂Cl₂P₂Pt
Molecular Weight:804.595
Hs Code.:

[((C<sub>6</sub>H<sub>5</sub>)3PCH<sub>2</sub>)((C<sub>6</sub>H<sub>5</sub>)3P)PtCl<sub>2</sub>]

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Chemical Property of [((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl₂]

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Technology Process of [((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl₂]

There total 1 articles about [((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl₂] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 81274-83-1
cis-[Pt(PPh₃)2(CH₂PPh₃)Cl]Cl

: 81191-75-5
[((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl₂]

Guidance literature:: In benzene; byproducts: P(C6H5)3; under Ar and in the dark, reflux of the starting complex in benzene at 80°C for 2 h; filtn., washed with benzene and pentane, dried in vac., elem. anal.;

Reference yield: 93.0%

: aluminium chloride dimer

: 81191-75-5
[((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl₂]

: 82438-14-0
[((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl]⁽¹⁺⁾*[AlCl₄]^(1-)=[((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl][AlCl₄]

Guidance literature:: In dichloromethane; (Ar); stirred for 2 h; centrifuged, evapd. (vac.), washed with CHCl3 and pentane, dried (vac.); elem. anal.;
DOI:10.1016/S0022-328X(00)84334-X

Reference yield:

: 81191-75-5
[((C₆H₅)3PCH₂)((C₆H₅)3P)PtCl₂]

: 81274-83-1
cis-[Pt(PPh₃)2(CH₂PPh₃)Cl]Cl

Guidance literature:: With triphenylphosphine; In dichloromethane; under Ar and in the dark, to the starting complex in CH2Cl2 addn. of P(C6H5)3, the mixt. is stirred (1 d, room temp.); evapn., washed with pentane;