6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside
CAS No.:117703-09-0
Molecular Formula:C₅₅H₇₂N₂O₁₈
Molecular Weight:1049.18
Hs Code.:

6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

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Chemical Property of 6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

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Technology Process of 6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 14 articles about 6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16697-49-7
3,4,6-tri-O-benzyl-1,2-O-(methoxyethylidene)-β-D-mannopyranose

: 117703-09-0
6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 45 percent / HgBr₂ / acetonitrile / 1.17 h / Heating

2: 85 percent / NaOMe / methanol / 4 h / Ambient temperature

3: 69 percent / borontrifluoride etherate / CH₂Cl₂ / 3.5 h / -8 °C

4: 70 percent / NH₃ in MeOH (sat.) / 40 h / Ambient temperature

5: NH₂NH₂ / ethanol / 3 h

6: 1) pyridine, 2) NH₃ in MeOH (sat.) / 1) 10 h, RT, 2) 44 h, RT

With pyridine; boron trifluoride diethyl etherate; ammonia; sodium methylate; mercury dibromide; hydrazine; In methanol; ethanol; dichloromethane; acetonitrile;

Reference yield:

: 3254-16-8,4435-05-6,19189-54-9,29748-21-8,50801-29-1,64727-26-0,64727-27-1,65338-02-5,67672-68-8,78418-55-0,80877-03-8,103002-27-3,103002-29-5,132562-62-0
3,4,6-tri-O-acetyl-1,2-O-(1-methoxyethylidene)-β-D-mannopyranose

: 117703-09-0
6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: 1) NH₃ in MeOH (sat.), 2) NaH / 1) 48 h, RT, 2) DMF, 3) DMF, 18 h, RT

2: 45 percent / HgBr₂ / acetonitrile / 1.17 h / Heating

3: 85 percent / NaOMe / methanol / 4 h / Ambient temperature

4: 69 percent / borontrifluoride etherate / CH₂Cl₂ / 3.5 h / -8 °C

5: 70 percent / NH₃ in MeOH (sat.) / 40 h / Ambient temperature

6: NH₂NH₂ / ethanol / 3 h

7: 1) pyridine, 2) NH₃ in MeOH (sat.) / 1) 10 h, RT, 2) 44 h, RT

With pyridine; boron trifluoride diethyl etherate; ammonia; sodium methylate; sodium hydride; mercury dibromide; hydrazine; In methanol; ethanol; dichloromethane; acetonitrile;

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 117703-09-0
6-(N-benzyloxycarbonylamino)-hexyl 2-O-(4-O-β-D-galactopyranosyl-2-acetamido-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / 1N NaOH / tetrahydrofuran / 4 °C

2: 45 percent / HgBr₂ / acetonitrile / 1.17 h / Heating

3: 85 percent / NaOMe / methanol / 4 h / Ambient temperature

4: 69 percent / borontrifluoride etherate / CH₂Cl₂ / 3.5 h / -8 °C

5: 70 percent / NH₃ in MeOH (sat.) / 40 h / Ambient temperature

6: NH₂NH₂ / ethanol / 3 h

7: 1) pyridine, 2) NH₃ in MeOH (sat.) / 1) 10 h, RT, 2) 44 h, RT

With pyridine; sodium hydroxide; boron trifluoride diethyl etherate; ammonia; sodium methylate; mercury dibromide; hydrazine; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;