C₈₁H₁₀₉NO₉

Base Information

Chemical Name:C₈₁H₁₀₉NO₉
CAS No.:947747-28-6
Molecular Formula:C₈₁H₁₀₉NO₉
Molecular Weight:1240.76
Hs Code.:

C<sub>81</sub>H<sub>109</sub>NO<sub>9</sub>

Synonyms:

Suppliers and Price of C₈₁H₁₀₉NO₉

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₈₁H₁₀₉NO₉

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₈₁H₁₀₉NO₉

There total 18 articles about C₈₁H₁₀₉NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947747-20-8
C₄₂H₄₀O₅

: 947747-28-6
C₈₁H₁₀₉NO₉

Guidance literature:: Multi-step reaction with 13 steps

1: 88 percent / pyridine

2: 94 percent / NaN₃ / dimethylformamide

3: 86 percent / PPTs / methanol

4: 64 percent / MeOTf / CH₂Cl₂

5: 81 percent / DDQ / CH₂Cl₂; methanol

6: 91 percent / TPAP; NMO; MS₄A / acetonitrile

7: 85 percent / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O

8: 90 percent / EDC*HCl / CH₂Cl₂

9: 80 percent / BuLi / tetrahydrofuran

10: 94 percent / (R)-B-Me-CBS; BH₃*SMe₂ / toluene

11: 87 percent / TBAI; NaH / dimethylformamide

12: NaBH₄ / tetrahydrofuran; methanol

13: pyridine

With sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; n-butyllithium; sodium azide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; dimethylsulfide borane complex; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; (R)-(+)-tetrahydro-1-methyl-1H,3H-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.05.161

Reference yield:

: 947747-21-9
C₄₂H₃₉N₃O₄

: 947747-28-6
C₈₁H₁₀₉NO₉

Guidance literature:: Multi-step reaction with 11 steps

1: 86 percent / PPTs / methanol

2: 64 percent / MeOTf / CH₂Cl₂

3: 81 percent / DDQ / CH₂Cl₂; methanol

4: 91 percent / TPAP; NMO; MS₄A / acetonitrile

5: 85 percent / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O

6: 90 percent / EDC*HCl / CH₂Cl₂

7: 80 percent / BuLi / tetrahydrofuran

8: 94 percent / (R)-B-Me-CBS; BH₃*SMe₂ / toluene

9: 87 percent / TBAI; NaH / dimethylformamide

10: NaBH₄ / tetrahydrofuran; methanol

11: pyridine

With sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; dimethylsulfide borane complex; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; (R)-(+)-tetrahydro-1-methyl-1H,3H-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.05.161

Reference yield:

: 947747-35-5
C₄₃H₄₂O₇S

: 947747-28-6
C₈₁H₁₀₉NO₉

Guidance literature:: Multi-step reaction with 12 steps

1: 94 percent / NaN₃ / dimethylformamide

2: 86 percent / PPTs / methanol

3: 64 percent / MeOTf / CH₂Cl₂

4: 81 percent / DDQ / CH₂Cl₂; methanol

5: 91 percent / TPAP; NMO; MS₄A / acetonitrile

6: 85 percent / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O

7: 90 percent / EDC*HCl / CH₂Cl₂

8: 80 percent / BuLi / tetrahydrofuran

9: 94 percent / (R)-B-Me-CBS; BH₃*SMe₂ / toluene

10: 87 percent / TBAI; NaH / dimethylformamide

11: NaBH₄ / tetrahydrofuran; methanol

12: pyridine

With sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; n-butyllithium; sodium azide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; dimethylsulfide borane complex; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; (R)-(+)-tetrahydro-1-methyl-1H,3H-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.05.161