BOCAsnCys(Trit)OH

Base Information

Chemical Name:BOCAsnCys(Trit)OH
CAS No.:72287-47-9
Molecular Formula:C₃₁H₃₅N₃O₆S
Molecular Weight:577.701
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of BOCAsnCys(Trit)OH

Chemical Property:

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Technology Process of BOCAsnCys(Trit)OH

There total 2 articles about BOCAsnCys(Trit)OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7536-55-2
N-tert-butyloxycarbonylasparagine

: 72287-47-9
BOCAsnCys(Trit)OH

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, pyridine / dimethylformamide

2: 1.) bis(trimethylsilyl)acetamide, 2.) Et₃N, pyridine / 1.) DMF, 2.) DMF, a) -10 deg C, 1 h, b) 2 deg C, 18 h

With pyridine; bis-(trimethylsilyl)acetamide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1007/BF00631031

Reference yield:

: 2799-07-7
S-trityl-L-cysteine

: C₁₄H₂₄N₂O₆

: 72287-47-9
BOCAsnCys(Trit)OH

Guidance literature:: With pyridine; bis-(trimethylsilyl)acetamide; triethylamine; Yield given. Multistep reaction; 1.) DMF, 2.) DMF, a) -10 deg C, 1 h, b) 2 deg C, 18 h;
DOI:10.1007/BF00631031

Reference yield: 63.0%

: 21688-04-0
HProLeuGlyNH₂ hydrochloride

: 72287-47-9
BOCAsnCys(Trit)OH

: 90303-95-0
BOCAsnCys(Trit)ProLeuGlyNH₂

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 48h; Ambient temperature;
DOI:10.1007/BF00631032