1-Methyl-N-[(4-nitrophenyl)methylene]-5-(1H-pyrrol-1-yl)-1H-pyrazole-4-methanamine

Base Information

Chemical Name:1-Methyl-N-[(4-nitrophenyl)methylene]-5-(1H-pyrrol-1-yl)-1H-pyrazole-4-methanamine
CAS No.:156032-54-1
Molecular Formula:C₁₆H₁₅N₅O₂
Molecular Weight:309.327
Hs Code.:
DSSTox Substance ID:DTXSID701131265

Synonyms:DTXSID701131265;1-Methyl-N-[(4-nitrophenyl)methylene]-5-(1H-pyrrol-1-yl)-1H-pyrazole-4-methanamine;156032-54-1

Suppliers and Price of 1-Methyl-N-[(4-nitrophenyl)methylene]-5-(1H-pyrrol-1-yl)-1H-pyrazole-4-methanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Methyl-N-[(4-nitrophenyl)methylene]-5-(1H-pyrrol-1-yl)-1H-pyrazole-4-methanamine

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:309.12257474
Heavy Atom Count:23
Complexity:425

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(=C(C=N1)CN=CC2=CC=C(C=C2)[N+](=O)[O-])N3C=CC=C3

Technology Process of 1-Methyl-N-[(4-nitrophenyl)methylene]-5-(1H-pyrrol-1-yl)-1H-pyrazole-4-methanamine

There total 3 articles about 1-Methyl-N-[(4-nitrophenyl)methylene]-5-(1H-pyrrol-1-yl)-1H-pyrazole-4-methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 555-16-8
4-nitrobenzaldehdye

: 156032-53-0
4-aminomethyl-1-methyl-5-(1H-pyrrol-1-yl)-1H-pyrazole

: 156032-54-1
4-(p-nitrobenzylideneaminomethyl)-1-methyl-5-(1-pyrryl)pyrazole

Guidance literature:: In ethanol; for 15h; Heating;
DOI:10.1016/0223-5234(94)90041-8

Reference yield:

: 5334-41-8
5-amino-4-cyano-1-methylpyrazole

: 156032-54-1
4-(p-nitrobenzylideneaminomethyl)-1-methyl-5-(1-pyrryl)pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / acetic acid / 0.5 h / Heating

2: 69 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 78 percent / ethanol / 15 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; ethanol; acetic acid;
DOI:10.1016/0223-5234(94)90041-8

Reference yield:

: 146885-48-5
4-cyano-1-methyl-5-(1H-pyrrol-1-yl)-1H-pyrazole

: 156032-54-1
4-(p-nitrobenzylideneaminomethyl)-1-methyl-5-(1-pyrryl)pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

2: 78 percent / ethanol / 15 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; ethanol;
DOI:10.1016/0223-5234(94)90041-8