N-methyl-2'-<(2-cyanoethyl)thio>-butananilide

Base Information

Chemical Name:N-methyl-2'-<(2-cyanoethyl)thio>-butananilide
CAS No.:141401-36-7
Molecular Formula:C₂₆H₃₃N₃O₆S₂
Molecular Weight:547.697
Hs Code.:

N-methyl-2'-<(2-cyanoethyl)thio>-<N-methoxycarbonyl-5-(p-toluenesulfonyloxy)propylamino>butananilide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-2'-<(2-cyanoethyl)thio>-butananilide

Chemical Property:

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Technology Process of N-methyl-2'-<(2-cyanoethyl)thio>-butananilide

There total 6 articles about N-methyl-2'-<(2-cyanoethyl)thio>-butananilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141401-30-1
4-(3-Benzyloxy-propylamino)-butyric acid methyl ester

: 141401-36-7
N-methyl-2'-<(2-cyanoethyl)thio>-butananilide

Guidance literature:: Multi-step reaction with 6 steps

1: K₂CO₃ / tetrahydrofuran / 1.5 h / 5 °C

2: H₂ / 10percent Pd/C / methanol / 7 h / Ambient temperature

3: pyridine / 13 h / 0 - 5 °C

4: 0.5N NaOH / H₂O; methanol / 3 h / Ambient temperature

5: oxalyl chloride / benzene / a) RT, 30 min, b) 60 deg C, 1 h

6: K₂CO₃ / tetrahydrofuran

With pyridine; sodium hydroxide; oxalyl dichloride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; water; benzene;
DOI:10.1248/cpb.40.617

Reference yield:

: 141401-31-2
methyl N-<3-(benzyloxy)propyl>-N-methoxycarbonyl-4-aminobutyrate

: 141401-36-7
N-methyl-2'-<(2-cyanoethyl)thio>-butananilide

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 10percent Pd/C / methanol / 7 h / Ambient temperature

2: pyridine / 13 h / 0 - 5 °C

3: 0.5N NaOH / H₂O; methanol / 3 h / Ambient temperature

4: oxalyl chloride / benzene / a) RT, 30 min, b) 60 deg C, 1 h

5: K₂CO₃ / tetrahydrofuran

With pyridine; sodium hydroxide; oxalyl dichloride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; water; benzene;
DOI:10.1248/cpb.40.617

Reference yield:

: 4-[(3-Hydroxy-propyl)-methoxycarbonyl-amino]-butyric acid methyl ester

: 141401-36-7
N-methyl-2'-<(2-cyanoethyl)thio>-butananilide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 13 h / 0 - 5 °C

2: 0.5N NaOH / H₂O; methanol / 3 h / Ambient temperature

3: oxalyl chloride / benzene / a) RT, 30 min, b) 60 deg C, 1 h

4: K₂CO₃ / tetrahydrofuran

With pyridine; sodium hydroxide; oxalyl dichloride; potassium carbonate; In tetrahydrofuran; methanol; water; benzene;
DOI:10.1248/cpb.40.617