bis(ethylbenzene)vanadium tris[tris(pentafluorophenyl)germyl]mercurate

Base Information

• Chemical Name: bis(ethylbenzene)vanadium tris[tris(pentafluorophenyl)germyl]mercurate
• CAS No.: 91581-94-1
• Molecular Formula: C₁₆H₂₀V*C₅₄F₄₅Ge₃Hg
• Molecular Weight: 2185.16
• Mol file: 91581-94-1.mol

Synonyms:

Chemical Property of bis(ethylbenzene)vanadium tris[tris(pentafluorophenyl)germyl]mercurate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(ethylbenzene)vanadium tris[tris(pentafluorophenyl)germyl]mercurate

There total 1 articles about bis(ethylbenzene)vanadium tris[tris(pentafluorophenyl)germyl]mercurate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.6%

bis(ethylbenzene)vanadium (36955-48-3) + bis[tris(pentafluorophenyl)germyl]mercury (35406-49-6) → bis(ethylbenzene)vanadium tris[tris(pentafluorophenyl)germyl]mercurate (91581-94-1)

Guidance literature:

In diethyl ether; byproducts: Hg; V compd. soln. added to Hg compd. soln., reacted for 5-10 h at 20°C; org. layer decanted from Hg, evapd. (vac.), washed with pentane, dried in vac.; elem. anal.;

DOI:10.1016/0022-328X(84)85006-8

Reference yield:

bis(ethylbenzene)vanadium tris[tris(pentafluorophenyl)germyl]mercurate (91581-94-1) → bis(ethylbenzene)vanadium (36955-48-3) + mercury

Guidance literature:

In tetrahydrofuran; Electrolysis; electrolysis of complex in THF;

DOI:10.1016/0022-328X(84)85006-8

upstream raw materials:

bis(ethylbenzene)vanadium

bis[tris(pentafluorophenyl)germyl]mercury

Downstream raw materials:

bis(ethylbenzene)vanadium