dimethyl(bis(diphenilphosphine)amine-κP,κP)platinum(II)

Base Information

Chemical Name:dimethyl(bis(diphenilphosphine)amine-κP,κP)platinum(II)
CAS No.:525602-28-2
Molecular Formula:C₂₆H₂₇NP₂Pt
Molecular Weight:610.535
Hs Code.:

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Chemical Property of dimethyl(bis(diphenilphosphine)amine-κP,κP)platinum(II)

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Technology Process of dimethyl(bis(diphenilphosphine)amine-κP,κP)platinum(II)

There total 11 articles about dimethyl(bis(diphenilphosphine)amine-κP,κP)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 151264-44-7
[PtCl₂(bis(diphenylphosphino)amine-P,P')]

: 917-54-4
methyllithium

: 525602-28-2
dimethyl(bis(diphenilphosphine)amine-κP,κP)platinum(II)

Guidance literature:: In diethyl ether; under Ar; a soln. of MeLi was slowly added to a stirred ice-cold soln. of Pt-contg. compd. (0.514 mmol) in dry ether; stiring for 2 h; the mixt. was hydrolyzed with water; sepn. of the org. layer, extn. withCH2Cl2, drying over MgSO4, evapn. of the org. solvents; the complex was washed with ether and dried under vac.; elem. anal.;
DOI:10.1039/b700009j

Reference yield: 30.0%

: bis[dimethyl(μ-dimethylsulfide)platinum(II)]

: 941670-73-1
[Pt(p-MeC₆H₄)2(bis(diphenylphosphino)amine-P)2]

: 525602-28-2
dimethyl(bis(diphenilphosphine)amine-κP,κP)platinum(II)

Guidance literature:: In benzene; Pt-contg. compd. (0.174 mmol) and Pt2-contg. compd. (0.087 mmol) in dry benzene was stirred at room temp. for 1 h; the solvent was removed and the compds. were washed with n-hexane and dried under vac.;
DOI:10.1039/b700009j

Reference yield:

: 2960-37-4
Bis(diphenylphosphanyl)amine

: 525602-28-2
dimethyl(bis(diphenilphosphine)amine-κP,κP)platinum(II)

Guidance literature:: Multi-step reaction with 3 steps

1: benzene

2: benzene

3: benzene-d6

In benzene-d6; benzene;
DOI:10.1039/b301419c