{(S)-2-(4-Hydroxy-phenyl)-1-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester

Base Information

• Chemical Name: {(S)-2-(4-Hydroxy-phenyl)-1-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester
• CAS No.: 89661-82-5
• Molecular Formula: C₃₆H₄₅N₅O₇
• Molecular Weight: 659.783

Synonyms:

Chemical Property of {(S)-2-(4-Hydroxy-phenyl)-1-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of {(S)-2-(4-Hydroxy-phenyl)-1-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester

There total 2 articles about {(S)-2-(4-Hydroxy-phenyl)-1-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine (78330-94-6) + D-α-phenylethylamine (98-84-0,618-36-0,2627-86-3,3886-69-9) → {(S)-2-(4-Hydroxy-phenyl)-1-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester (89661-82-5,89708-71-4)

Guidance literature:

With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; 1.) 1 h, -10 deg C, 2.) 1-2 h, 0-10 deg C;

Reference yield:

N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine (78330-94-6) + L-α-phenylethylamine (98-84-0,618-36-0,2627-86-3,3886-69-9) → {(S)-2-(4-Hydroxy-phenyl)-1-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester (89661-82-5,89708-71-4)

Guidance literature:

With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; 1.) 1 h, -10 deg C, 2.) 1-2 h, 0-10 deg C;

Reference yield:

{(S)-2-(4-Hydroxy-phenyl)-1-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethylcarbamoyl]-ethyl}-carbamic acid tert-butyl ester (89661-82-5,89708-71-4) → H-Tyr-D-Ala-Phe-Gly-D-NH-CH(CH3)C6H5 (83603-32-1)

Guidance literature:

With methoxybenzene; trifluoroacetic acid; for 0.5h; Yield given;

upstream raw materials:

N-Boc-L-tyrosyl-D-alanyl-L-phenylalanyl-glycine

D-α-phenylethylamine

L-α-phenylethylamine

Downstream raw materials:

H-Tyr-D-Ala-Phe-Gly-D-NH-CH(CH₃)C₆H₅

(S)-2-Amino-3-(4-hydroxy-phenyl)-N-[(R)-1-((S)-2-phenyl-1-{[(1-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-ethylcarbamoyl)-ethyl]-propionamide

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