diphenyltin bis(hydroxyethanethiolate)

Base Information

• Chemical Name: diphenyltin bis(hydroxyethanethiolate)
• CAS No.: 78899-73-7
• Molecular Formula: C₁₆H₂₀O₂S₂Sn
• Molecular Weight: 427.176

Synonyms:

Chemical Property of diphenyltin bis(hydroxyethanethiolate)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of diphenyltin bis(hydroxyethanethiolate)

There total 1 articles about diphenyltin bis(hydroxyethanethiolate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

diphenyltin oxide + 2-hydroxyethanethiol (60-24-2) → diphenyltin bis(hydroxyethanethiolate) (78899-73-7)

Guidance literature:

In chloroform; byproducts: H2O; treatment of freshly prepared stannoxane with 2 equiv. thiol until dissoln. (slight warming); drying (Na2SO4), partial evapn. (reduced pressure, 10°C), addn. of petroleum ether, cooling (refrigerator, overnight), washing (petroleum ether/Et2O=1:1), drying (vac., 10°C); elem. anal.;

DOI:10.1016/S0020-1693(00)90455-9

Reference yield:

diphenyltin bis(hydroxyethanethiolate) (78899-73-7) → Sn(4+)*2C6H5(1-)*SCH2CH2O(2-)=(C6H5)2Sn(SCH2CH2O)

Guidance literature:

In neat (no solvent); byproducts: HSCH2CH2OH; 30°C, several days (or room temp., prolonged reaction time);

DOI:10.1016/S0020-1693(00)90455-9

upstream raw materials:

2-hydroxyethanethiol

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