[(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]Li

Base Information

Chemical Name:[(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]Li
CAS No.:1030903-40-2
Molecular Formula:C₂₅H₃₉ClN₂PPt*Li
Molecular Weight:636.046
Hs Code.:

[(NC<sub>5</sub>H<sub>3</sub>-2-(CHP(t-Bu)2)(CH<sub>2</sub>NEt<sub>2</sub>))Pt(Cl)(C<sub>6</sub>H<sub>5</sub>)]Li

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Chemical Property of [(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]Li

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Technology Process of [(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]Li

There total 2 articles about [(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]Li which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: [(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))PtCl]*0.5C₆H₆

: 591-51-5
phenyllithium

: 1030903-40-2
[(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]Li

Guidance literature:: In tetrahydrofuran; (N2); Schlenk technique; soln. of PhLi in THF was added to soln. of Pt complex in THF; NMR monitoring; solvent removed (vac., 1 h); extd. (C6H6); evapd.;
DOI:10.1021/om8001069

Reference yield:

: 1030903-38-8
[(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(CH₃)]Li

: 1030903-40-2
[(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]Li

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran-d8

2: tetrahydrofuran

In tetrahydrofuran; tetrahydrofuran-d8;
DOI:10.1021/om8001069

Reference yield: 71.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 1030903-40-2
[(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]Li

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: [(NC₅H₃-2-(CHP(t-Bu)2)(CH₂NEt₂))PtCl]*0.5C₆H₆

: [(NC₅H₃-2-(CH₂P(t-Bu)2)(CH₂NEt₂))Pt(Cl)(C₆H₅)]*C₆H₆

Guidance literature:: In tetrahydrofuran; 1,4-dioxane; (N2); Schlenk technique; soln. of HCl in dioxane was added to soln. of Pt complex in THF at room temp.; NMR monitoring; solvent removed (vac.); extd. (pentane); evapd.; elem. anal.;
DOI:10.1021/om8001069