W₂Ph₂(MeCCMe)2(O-i-Pr)4

Base Information

Chemical Name:W₂Ph₂(MeCCMe)2(O-i-Pr)4
CAS No.:116563-30-5
Molecular Formula:C₃₂H₅₀O₄W₂
Molecular Weight:866.447
Hs Code.:

W<sub>2</sub>Ph<sub>2</sub>(MeCCMe)2(O-i-Pr)4

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of W₂Ph₂(MeCCMe)2(O-i-Pr)4

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Technology Process of W₂Ph₂(MeCCMe)2(O-i-Pr)4

There total 1 articles about W₂Ph₂(MeCCMe)2(O-i-Pr)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 503-17-3
dimethylacetylene

: 101915-85-9
W₂(C₆H₅)2(O-i-Pr)4(HNMe₂)

: 116563-30-5
W₂Ph₂(MeCCMe)2(O-i-Pr)4

Guidance literature:: In pentane; W2(C6H5)2(O-i-Pr)4(HNMe2)/pentane was frozen to -198°C, then addn. of 2.0 equiv. 2-butyne; warmed rapidly to 0°C; stirred 5min., cooled to -20°C for 48h; removing of the supernatant liquid, dried in vacuo; detected by NMR and X-ray diffraction;